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@INPROCEEDINGS{Izumoto:859328,
author = {Izumoto, Satoshi and Huisman, Johan Alexander and
Zimmermann, Egon and Méheust, Yves and Gomez, Francesco and
Heyman, Joris and Wu, Yuxin and Vereecken, Harry and Le
Borgne, Tanguy},
title = {{S}pectral induced polarization of calcite precipitation in
a porous media},
reportid = {FZJ-2019-00197},
year = {2018},
abstract = {Induced calcite precipitation is used in a range of in-situ
geotechnical applications to modify the mechanical and
hydrological properties of soils and fractured rocks. It is
also a model process for mixing-induced biogeochemical
reactions that occur naturally in a broad range of
hydrological systems. Laboratory experiments have shown that
spectral induced polarization (SIP) measurements can be used
to monitor calcite precipitation. However, the results of
the limited number of previous studies investigating the SIP
response of calcite precipitation were not fully consistent.
This study aims to investigate how the SIP response of
calcite depends on solute composition, since this may
explain the differences in SIP response observed in previous
studies. For this, a five-phase experiment with SIP
measurements on a column filled with sand was performed. In
phase I, calcite precipitation was generated for a period of
12 days by injecting Na2CO3 and CaCl2 solutions through two
different ports. This resulted in a well-defined calcite
precipitation front, which was associated with an increase
in the imaginary conductivity in the kHz frequency range. In
phase II, the injected solutions were stepwise diluted. This
resulted in a clear decrease in the imaginary conductivity.
In phase III, the injection of the two solutions was
stopped. Nevertheless, calcite precipitation continued and
solute concentrations in the mixing zone decreased. As in
phase II, this led to a decrease in the imaginary
conductivity. In phase IV, the injection rate of the Na2CO3
solution was reduced to shift the mixing zone away from the
calcite precipitation front, which also decreased the
imaginary conductivity. Finally, the column was flushed with
a solution in equilibrium with calcite in phase V, which led
to a very small SIP signal. These results imply that the SIP
response of calcite is very sensitive to the solution
composition near the precipitates, which may explain the
previously reported conflicting results. In a next step, the
relationship between SIP response, volume of calcite, and
solute composition will be quantitatively investigated using
SIP measurements on a 2D milifluidic cell with an artificial
porous media that allows visualizing the temporal dynamics
of calcite precipitation.},
month = {Dec},
date = {2018-12-10},
organization = {AGU Fall Meeting, Washington, D.C.
(USA), 10 Dec 2018 - 14 Dec 2018},
subtyp = {After Call},
cin = {IBG-3 / ZEA-2},
cid = {I:(DE-Juel1)IBG-3-20101118 / I:(DE-Juel1)ZEA-2-20090406},
pnm = {255 - Terrestrial Systems: From Observation to Prediction
(POF3-255) / ENIGMA - European training Network for In situ
imaGing of dynaMic processes in heterogeneous subsurfAce
environments (722028)},
pid = {G:(DE-HGF)POF3-255 / G:(EU-Grant)722028},
typ = {PUB:(DE-HGF)24},
url = {https://juser.fz-juelich.de/record/859328},
}