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@ARTICLE{Thoma:859469,
author = {Thoma, Henrik and Luberstetter, Wolfgang and Peters,
Jürgen and Hutanu, Vladimir},
title = {{P}olarized neutron diffraction using a novel high-{T}c
superconducting magnet on the single-crystal diffractometer
{POLI} at {MLZ}},
journal = {Journal of applied crystallography},
volume = {51},
number = {1},
issn = {1600-5767},
address = {[S.l.]},
publisher = {Wiley-Blackwell},
reportid = {FZJ-2019-00325},
pages = {17 - 26},
year = {2018},
abstract = {The polarized single-crystal diffractometer POLI is the
first neutron scattering instrument routinely using 3 He
spin filters both to produce and to analyse neutron
polarization. The instrument, with a non-magnetic
goniometer, was designed to perform two types of polarized
neutron diffraction experiment: spherical neutron
polarimetry, also known as full three-dimensional
polarization analysis in zero magnetic field, and classical
polarized neutron diffraction, also called the
flipping-ratio (FR) method, in high applied magnetic fields.
Reported here is the implementation of the FR setup for
short-wavelength neutrons on POLI using a new high- T c
superconducting magnet with a maximal field of 2.2 T. The
complete setup consists of a 3 He polarizer, a nutator, a
Mezei-type flipper, guide fields and dedicated pole pieces,
together with the magnet. Each component, as well as the
whole setup, was numerically simulated, optimized, built and
finally successfully tested under real experimental
conditions on POLI. The measured polarized neutron spin
transport efficiency is about $99\%$ at different
wavelengths, e.g. as short as 0.7 Å, and up to the maximal
available field of the magnet. No further depolarization of
the 3 He cells due to stray fields of the magnet occurs. The
additional use of the available 3 He analyser allows
uniaxial polarization analysis experiments in fields up to
1.2 T. The results of the first experiment on the
field-dependent distribution of the trigonal
antiferromagnetic domains in haematite (α-Fe 2 O 3 ) are
presented and compared with the literature data.},
cin = {JCNS-FRM-II / JCNS-2},
ddc = {540},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-2-20110106},
pnm = {524 - Controlling Collective States (POF3-524) / 6G15 - FRM
II / MLZ (POF3-6G15) / 6G4 - Jülich Centre for Neutron
Research (JCNS) (POF3-623) / 6212 - Quantum Condensed
Matter: Magnetism, Superconductivity (POF3-621)},
pid = {G:(DE-HGF)POF3-524 / G:(DE-HGF)POF3-6G15 /
G:(DE-HGF)POF3-6G4 / G:(DE-HGF)POF3-6212},
experiment = {EXP:(DE-MLZ)POLI-HEIDI-20140101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000424121500003},
doi = {10.1107/S160057671800078X},
url = {https://juser.fz-juelich.de/record/859469},
}