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@ARTICLE{Simonenko:859746,
      author       = {Simonenko, Elizaveta P. and Simonenko, Nikolay P. and
                      Kopitsa, Gennady P. and Mokrushin, Artem S. and Khamova,
                      Tamara V. and Sizova, Svetlana V. and Khaddazh, Mishal and
                      Tsvigun, Natalia V. and Pipich, Vitaliy and Gorshkova, Yulia
                      E. and Sevastyanov, Vladimir G. and Kuznetsov, Nikolay T.},
      title        = {{A} sol-gel synthesis and gas-sensing properties of finely
                      dispersed {Z}r{T}i{O}4},
      journal      = {Materials chemistry and physics},
      volume       = {225},
      issn         = {0254-0584},
      address      = {New York, NY [u.a.]},
      publisher    = {Elsevier},
      reportid     = {FZJ-2019-00583},
      pages        = {347 - 357},
      year         = {2019},
      abstract     = {The transparent titanium-zirconium-containing gel was
                      obtained using heteroligand coordination compounds (namely,
                      alkoxoacetylacetonates) as the precursors. The
                      high-dispersive system “ZrTiO4 – carbon”, formed after
                      drying of such gel and carbonization of the obtained
                      xerogel, was used to study the evolution of microstructure
                      for the product (ZrTiO4) during thermal treatment in air for
                      1 h in the temperature range from 500 °C to 1000°С. It
                      was stated that the formation of crystalline phase occurred
                      in the narrow range 690-730°С. The thermal treatment at
                      500 °C and 600°С allowed obtaining micro- and mesoporous
                      X-ray amorphous products of the composition ZrTiO4, with the
                      specific surface area falling in the range 82–150m2/g. At
                      the higher temperatures the single-phase nanocrystalline
                      powder was prepared (the specific surface area amounted to
                      2.5–15m2/g). Particle coarsening took place more
                      extensively at temperatures ≥700°С was shown. For the
                      ZrTiO4 nanopowder crystallized under the mildest conditions
                      at the temperature of 700 °C, chemoresistive gas-sensitive
                      properties were studied for the first time. The material
                      showed a high reproducible response at $1–20\%$ O2 and
                      200–10,000 ppm H2 at a relatively low detection operating
                      temperature of 450 °C.},
      cin          = {JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
      ddc          = {530},
      cid          = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
                      I:(DE-Juel1)JCNS-1-20110106},
      pnm          = {6G4 - Jülich Centre for Neutron Research (JCNS) (POF3-623)
                      / 6G15 - FRM II / MLZ (POF3-6G15)},
      pid          = {G:(DE-HGF)POF3-6G4 / G:(DE-HGF)POF3-6G15},
      experiment   = {EXP:(DE-MLZ)KWS3-20140101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000463847900047},
      doi          = {10.1016/j.matchemphys.2018.12.102},
      url          = {https://juser.fz-juelich.de/record/859746},
}