Hauptseite > Publikationsdatenbank > A sol-gel synthesis and gas-sensing properties of finely dispersed ZrTiO4 > print

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024 7 _ |a 10.1016/j.matchemphys.2018.12.102
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024 7 _ |a 1879-3312
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037 _ _ |a FZJ-2019-00583
041 _ _ |a English
082 _ _ |a 530
100 1 _ |a Simonenko, Elizaveta P.
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245 _ _ |a A sol-gel synthesis and gas-sensing properties of finely dispersed ZrTiO4
260 _ _ |a New York, NY [u.a.]
|c 2019
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336 7 _ |a article
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520 _ _ |a The transparent titanium-zirconium-containing gel was obtained using heteroligand coordination compounds (namely, alkoxoacetylacetonates) as the precursors. The high-dispersive system “ZrTiO4 – carbon”, formed after drying of such gel and carbonization of the obtained xerogel, was used to study the evolution of microstructure for the product (ZrTiO4) during thermal treatment in air for 1 h in the temperature range from 500 °C to 1000°С. It was stated that the formation of crystalline phase occurred in the narrow range 690-730°С. The thermal treatment at 500 °C and 600°С allowed obtaining micro- and mesoporous X-ray amorphous products of the composition ZrTiO4, with the specific surface area falling in the range 82–150m2/g. At the higher temperatures the single-phase nanocrystalline powder was prepared (the specific surface area amounted to 2.5–15m2/g). Particle coarsening took place more extensively at temperatures ≥700°С was shown. For the ZrTiO4 nanopowder crystallized under the mildest conditions at the temperature of 700 °C, chemoresistive gas-sensitive properties were studied for the first time. The material showed a high reproducible response at 1–20% O2 and 200–10,000 ppm H2 at a relatively low detection operating temperature of 450 °C.
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700 1 _ |a Simonenko, Nikolay P.
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700 1 _ |a Kopitsa, Gennady P.
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700 1 _ |a Mokrushin, Artem S.
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700 1 _ |a Khamova, Tamara V.
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700 1 _ |a Sizova, Svetlana V.
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700 1 _ |a Khaddazh, Mishal
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700 1 _ |a Tsvigun, Natalia V.
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700 1 _ |a Gorshkova, Yulia E.
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700 1 _ |a Sevastyanov, Vladimir G.
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700 1 _ |a Kuznetsov, Nikolay T.
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773 _ _ |a 10.1016/j.matchemphys.2018.12.102
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