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@INPROCEEDINGS{Lobe:860155,
author = {Lobe, Sandra and Dellen, Christian and Windmüller, Anna
and Tsai, Chih-Long and Möller, Sören and Sohn, Yoo Jung
and Sebold, Doris and Finsterbusch, Martin and
Fattakhova-Rohlfing, Dina and Uhlenbruck, Sven and Guillon,
Olivier},
title = {{T}hin film electrolytes for all-solid-state lithium
batteries by sputter deposition},
reportid = {FZJ-2019-00941},
year = {2018},
abstract = {Current battery research and development is focused on
cells with high energy density as well as high inherent
safety. One approach to reach both goals at the same time is
a battery concept including a mixed cathode, a solid-state
thin film electrolyte and a lithium metal anode.
Lithium-stuffed garnets, like Li7La3Zr2O12 (LLZ), are
promising electrolyte materials due to their high ionic
conductivity and chemical and electrochemical stability with
Lithium and common cathode materials, e.g. LiCoO2. However,
the co-sintering of garnets with cathode material is impeded
by the low thermal stability of these mixtures (e.g. <700°C
for LiCoO2, <600°C for 5 V lithium manganese based
spinels). Well-defined interfaces can be obtained, when the
electrolyte is processed via gas phase at significant lower
temperatures than in co-sintering processes. In a previous
study we showed that single-phase LLZ thin films with a
Li-ion conductivity of 1.2x10-4 S cm-1 can be formed by a
sputter deposition process at 700°C. However, this
deposition temperature leads to interphase formation with
the used substrate material.In order to avoid detrimental
diffusion and reaction during deposition, our approach
concentrates on the reduction of substrate temperature by
careful adjustment of the process parameters. Furthermore,
the microstructure of the thin films has to be optimized, so
that the Li-ion conductivity can be maximized. Therefore,
post-annealing in different atmospheres was applied, too. As
a major result we will show the deposition of
garnet-structured thin films at around 400°C. The
integration of garnet electrolytes in all-solid-state
lithium batteries is facilitated by this low deposition
temperature. That means, even electrodes, that show a low
thermal stability, like e.g. high-voltage spinel materials,
could be used as substrate for deposition of garnet
electrolytes.},
month = {Jan},
date = {2018-01-24},
organization = {Batterieforum Deutschland, Berlin
(Germany), 24 Jan 2018 - 26 Jan 2018},
subtyp = {After Call},
cin = {IEK-1},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)24},
url = {https://juser.fz-juelich.de/record/860155},
}