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@ARTICLE{Nlle:860247,
author = {Nölle, Roman and Achazi, Andreas J. and Kaghazchi, Payam
and Winter, Martin and Placke, Tobias},
title = {{P}entafluorophenyl {I}socyanate as an {E}ffective
{E}lectrolyte {A}dditive for {I}mproved {P}erformance of
{S}ilicon-{B}ased {L}ithium-{I}on {F}ull {C}ells},
journal = {ACS applied materials $\&$ interfaces},
volume = {10},
number = {33},
issn = {1944-8252},
address = {Washington, DC},
publisher = {Soc.},
reportid = {FZJ-2019-01031},
pages = {28187 - 28198},
year = {2018},
abstract = {Due to its high specific and volumetric capacity and
relatively low operation potential, silicon (Si) has
attracted much attention to be utilized as a high-capacity
anode material for lithium-ion batteries (LIBs) with
increased energy density. However, the application of Si
within commercial LIBs is still hindered by its poor cycling
stability related to the huge volume changes of Si upon
lithiation/delithiation, followed by continuous electrolyte
decomposition and active lithium loss at the anode side. In
this work, we present the application of pentafluorophenyl
isocyanate (PFPI) as an effective electrolyte additive for
lithium-ion full cells, containing a pure,
magnetron-sputtered Si anode and a LiNi1/3Mn1/3Co1/3O2
(NMC-111) cathode. The performance of the Si/NMC-111 full
cells is significantly improved in terms of capacity
retention and Coulombic efficiency by the addition of 2 wt
$\%$ PFPI to the baseline electrolyte and is compared to the
well-known additives vinylene carbonate and fluoroethylene
carbonate. Furthermore, it is revealed that the additive is
able to reduce the active lithium losses by forming an
effective solid–electrolyte interphase (SEI) on the Si
anode. X-ray photoelectron spectroscopy investigations
unveil that PFPI is a main part of the SEI layer, leading to
less active lithium immobilized within the interphase.
Overall, our results pave the path for a broad range of
different isocyanate compounds, which have not been studied
for Si-based anodes in lithium-ion full cells so far. These
compounds can be easily adjusted by modifying the chemical
structure and/or functional groups incorporated within the
molecule, to specifically tailor the SEI layer for Si-based
anodes in LIBs.},
cin = {IEK-1},
ddc = {600},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:30044617},
UT = {WOS:000442706600068},
doi = {10.1021/acsami.8b07683},
url = {https://juser.fz-juelich.de/record/860247},
}