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000861054 1001_ $$00000-0002-3288-2795$$aSiebels, Marvin$$b0
000861054 245__ $$aSynthesis of rare-earth metal and rare-earth metal-fluoride nanoparticles in ionic liquids and propylene carbonate
000861054 260__ $$aFrankfurt, M.$$bBeilstein-Institut zur Förderung der Chemischen Wissenschaften$$c2018
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000861054 520__ $$aDecomposition of rare-earth tris(N,N′-diisopropyl-2-methylamidinato)metal(III) complexes [RE{MeC(N(iPr)2)}3] (RE(amd)3; RE = Pr(III), Gd(III), Er(III)) and tris(2,2,6,6-tetramethyl-3,5-heptanedionato)europium(III) (Eu(dpm)3) induced by microwave heating in the ionic liquids (ILs) 1-butyl-3-methylimidazolium tetrafluoroborate ([BMIm][BF4]), 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide ([BMIm][NTf2]) and in propylene carbonate (PC) yield oxide-free rare-earth metal nanoparticles (RE-NPs) in [BMIm][NTf2] and PC for RE = Pr, Gd and Er or rare-earth metal-fluoride nanoparticles (REF3-NPs) in the fluoride-donating IL [BMIm][BF4] for RE = Pr, Eu, Gd and Er. The crystalline phases and the absence of significant oxide impurities in RE-NPs and REF3-NPs were verified by powder X-ray diffraction (PXRD), selected area electron diffraction (SAED) and high-resolution X-ray photoelectron spectroscopy (XPS). The size distributions of the nanoparticles were determined by transmission electron microscopy (TEM) and high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM) to an average diameter of (11 ± 6) to (38 ± 17) nm for the REF3-NPs from [BMIm][BF4]. The RE-NPs from [BMIm][NTf2] or PC showed diameters of (1.5 ± 0.5) to (5 ± 1) nm. The characterization was completed by energy-dispersive X-ray spectroscopy (EDX).
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000861054 7001_ $$00000-0001-8949-0736$$aMai, Lukas$$b1
000861054 7001_ $$00000-0002-2369-9331$$aSchmolke, Laura$$b2
000861054 7001_ $$0P:(DE-HGF)0$$aSchütte, Kai$$b3
000861054 7001_ $$0P:(DE-Juel1)130525$$aBarthel, Juri$$b4
000861054 7001_ $$0P:(DE-HGF)0$$aYue, Junpei$$b5
000861054 7001_ $$0P:(DE-Juel1)130168$$aThomas, Jörg$$b6
000861054 7001_ $$0P:(DE-HGF)0$$aSmarsly, Bernd M$$b7
000861054 7001_ $$00000-0003-2142-8105$$aDevi, Anjana$$b8
000861054 7001_ $$00000-0002-7532-5286$$aFischer, Roland A$$b9
000861054 7001_ $$00000-0002-6288-9605$$aJaniak, Christoph$$b10$$eCorresponding author
000861054 773__ $$0PERI:(DE-600)2583584-1$$a10.3762/bjnano.9.180$$gVol. 9, p. 1881 - 1894$$p1881 - 1894$$tBeilstein journal of nanotechnology$$v9$$x2190-4286$$y2018
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