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| 001 | 861054 | ||
| 005 | 20210130000709.0 | ||
| 024 | 7 | _ | |a 10.3762/bjnano.9.180 |2 doi |
| 024 | 7 | _ | |a 2128/21718 |2 Handle |
| 024 | 7 | _ | |a pmid:30013882 |2 pmid |
| 024 | 7 | _ | |a WOS:000436839900001 |2 WOS |
| 037 | _ | _ | |a FZJ-2019-01638 |
| 082 | _ | _ | |a 620 |
| 100 | 1 | _ | |a Siebels, Marvin |0 0000-0002-3288-2795 |b 0 |
| 245 | _ | _ | |a Synthesis of rare-earth metal and rare-earth metal-fluoride nanoparticles in ionic liquids and propylene carbonate |
| 260 | _ | _ | |a Frankfurt, M. |c 2018 |b Beilstein-Institut zur Förderung der Chemischen Wissenschaften |
| 336 | 7 | _ | |a article |2 DRIVER |
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| 336 | 7 | _ | |a Journal Article |0 0 |2 EndNote |
| 520 | _ | _ | |a Decomposition of rare-earth tris(N,N′-diisopropyl-2-methylamidinato)metal(III) complexes [RE{MeC(N(iPr)2)}3] (RE(amd)3; RE = Pr(III), Gd(III), Er(III)) and tris(2,2,6,6-tetramethyl-3,5-heptanedionato)europium(III) (Eu(dpm)3) induced by microwave heating in the ionic liquids (ILs) 1-butyl-3-methylimidazolium tetrafluoroborate ([BMIm][BF4]), 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide ([BMIm][NTf2]) and in propylene carbonate (PC) yield oxide-free rare-earth metal nanoparticles (RE-NPs) in [BMIm][NTf2] and PC for RE = Pr, Gd and Er or rare-earth metal-fluoride nanoparticles (REF3-NPs) in the fluoride-donating IL [BMIm][BF4] for RE = Pr, Eu, Gd and Er. The crystalline phases and the absence of significant oxide impurities in RE-NPs and REF3-NPs were verified by powder X-ray diffraction (PXRD), selected area electron diffraction (SAED) and high-resolution X-ray photoelectron spectroscopy (XPS). The size distributions of the nanoparticles were determined by transmission electron microscopy (TEM) and high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM) to an average diameter of (11 ± 6) to (38 ± 17) nm for the REF3-NPs from [BMIm][BF4]. The RE-NPs from [BMIm][NTf2] or PC showed diameters of (1.5 ± 0.5) to (5 ± 1) nm. The characterization was completed by energy-dispersive X-ray spectroscopy (EDX). |
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| 700 | 1 | _ | |a Mai, Lukas |0 0000-0001-8949-0736 |b 1 |
| 700 | 1 | _ | |a Schmolke, Laura |0 0000-0002-2369-9331 |b 2 |
| 700 | 1 | _ | |a Schütte, Kai |0 P:(DE-HGF)0 |b 3 |
| 700 | 1 | _ | |a Barthel, Juri |0 P:(DE-Juel1)130525 |b 4 |
| 700 | 1 | _ | |a Yue, Junpei |0 P:(DE-HGF)0 |b 5 |
| 700 | 1 | _ | |a Thomas, Jörg |0 P:(DE-Juel1)130168 |b 6 |
| 700 | 1 | _ | |a Smarsly, Bernd M |0 P:(DE-HGF)0 |b 7 |
| 700 | 1 | _ | |a Devi, Anjana |0 0000-0003-2142-8105 |b 8 |
| 700 | 1 | _ | |a Fischer, Roland A |0 0000-0002-7532-5286 |b 9 |
| 700 | 1 | _ | |a Janiak, Christoph |0 0000-0002-6288-9605 |b 10 |e Corresponding author |
| 773 | _ | _ | |a 10.3762/bjnano.9.180 |g Vol. 9, p. 1881 - 1894 |0 PERI:(DE-600)2583584-1 |p 1881 - 1894 |t Beilstein journal of nanotechnology |v 9 |y 2018 |x 2190-4286 |
| 856 | 4 | _ | |y OpenAccess |u https://juser.fz-juelich.de/record/861054/files/2190-4286-9-180.pdf |
| 856 | 4 | _ | |y OpenAccess |x pdfa |u https://juser.fz-juelich.de/record/861054/files/2190-4286-9-180.pdf?subformat=pdfa |
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