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@ARTICLE{Weber:862397,
author = {Weber, Moritz L. and Baeumer, Christoph and Mueller, David
N. and Jin, Lei and Jia, Chun-Lin and Bick, Daniel S. and
Waser, R. and Dittmann, Regina and Valov, Ilia and Gunkel,
Felix},
title = {{E}lectrolysis of {W}ater at {A}tomically {T}ailored
{E}pitaxial {C}obaltite {S}urfaces},
journal = {Chemistry of materials},
volume = {31},
number = {7},
issn = {1520-5002},
address = {Washington, DC},
publisher = {American Chemical Society},
reportid = {FZJ-2019-02725},
pages = {2337 - 2346},
year = {2019},
abstract = {As complex transition-metal oxides of perovskite
structures, many cobaltites are active electrocatalysts
promoting oxygen evolution reaction (OER) during
electrochemical water splitting. To unveil specific
structure–activity relationships for electrocatalytic
performance, innovative types of catalysts are required to
overcome the inherent high complexity of regular powder
catalysts, where thin-film technology gained significance in
recent years. As we demonstrate, epitaxial La0.6Sr0.4CoO3
(LSCO) thin films can be deposited with controlled bulk
properties, surface structure, and stoichiometry on
orthorhombic (110) NdGaO3 single-crystalline substrates by
pulsed-laser deposition, providing ideal model systems for
this purpose. The epitaxial thin films are dense and single
crystalline with sub-nanometer surface roughness and grow
well oriented toward the pseudocubic [001] direction. The
LSCO thin films show high activity catalyzing the OER and
can carry significant current density loads exceeding 100
mA/cm2. Using these model catalysts, X-ray photoemission
spectroscopy reveals the degradation of the material under
these dynamic conditions, involving cation leaching and a
phase transformation of the oxide. An altered surface
stoichiometry as well as cobalt hydroxide formation is
observed. Our results show that epitaxial model systems can
be operated at large current density loads, allowing a
systematic study of catalysts and their degradation under
highly dynamic conditions.},
cin = {PGI-7 / JARA-FIT / PGI-6 / ER-C-1},
ddc = {540},
cid = {I:(DE-Juel1)PGI-7-20110106 / $I:(DE-82)080009_20140620$ /
I:(DE-Juel1)PGI-6-20110106 / I:(DE-Juel1)ER-C-1-20170209},
pnm = {524 - Controlling Collective States (POF3-524)},
pid = {G:(DE-HGF)POF3-524},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000464477100016},
doi = {10.1021/acs.chemmater.8b04577},
url = {https://juser.fz-juelich.de/record/862397},
}