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@ARTICLE{Dash:863293,
      author       = {Dash, Apurv and Sohn, Yoo Jung and Vaßen, Robert and
                      Guillon, Olivier and Gonzalez-Julian, Jesus},
      title        = {{S}ynthesis of {T}i3{S}i{C}2 {MAX} phase powder by a molten
                      salt shielded synthesis ({MS}3) method in air},
      journal      = {Journal of the European Ceramic Society},
      volume       = {39},
      number       = {13},
      issn         = {0955-2219},
      address      = {Amsterdam [u.a.]},
      publisher    = {Elsevier Science},
      reportid     = {FZJ-2019-03380},
      pages        = {3651-3659},
      year         = {2019},
      abstract     = {Titanium silicon carbide (Ti3SiC2) powder was synthesized
                      by molten salt shielded synthesis route of elemental
                      reactants. Potassium bromide (KBr) was used for gas-tight
                      encapsulation of the consolidated reaction mixture for
                      further high temperature processing. The synthesis of
                      Ti3SiC2 powder was carried out in air, the salt cladding and
                      molten salt pool provided for the protection of the material
                      against oxidation both at low and high temperature. The
                      process yielded free flowing Ti3SiC2 powders without the
                      need of a milling step. Al addition to the reaction mixture
                      resulted in a high purity (96 wt. $\%)$ of Ti3SiC2 at a
                      synthesis temperature of 1250 °C. The synthesized
                      micro-metric Ti3SiC2 can be milled to nano-metric powders.},
      cin          = {IEK-1},
      ddc          = {660},
      cid          = {I:(DE-Juel1)IEK-1-20101013},
      pnm          = {113 - Methods and Concepts for Material Development
                      (POF3-113)},
      pid          = {G:(DE-HGF)POF3-113},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000474678500015},
      doi          = {10.1016/j.jeurceramsoc.2019.05.011},
      url          = {https://juser.fz-juelich.de/record/863293},
}