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@ARTICLE{Zhang:863370,
author = {Zhang, Tong and Porcher, Willy and Paillard, Elie},
title = {{T}owards practical sulfolane based electrolytes: {C}hoice
of {L}i salt for graphite electrode operation},
journal = {Journal of power sources},
volume = {395},
issn = {0378-7753},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2019-03443},
pages = {212 - 220},
year = {2018},
abstract = {Sulfolane (tetramethylene sulfone, SL) is known for leading
to Li-ion electrolytes with high anodic stability. However,
the operation of graphite electrodes in alternative
electrolytes is usually challenging, especially when
ethylene carbonate (EC) is not used as co-solvent. Thus, we
study here the influence of the lithium salt on the
physico-chemical and electrochemical properties of EC-free
SL-based electrolytes and on the performance of graphite
electrodes based on carboxymethyl cellulose (CMC). SL mixed
with dimethyl carbonate (DMC) leads to electrolytes as
conductive as state-of-the-art alkyl carbonate-based
electrolytes with wide electrochemical stability windows.
The compatibility with graphite electrodes depends on the Li
salt used and, even though cycling is possible with most
salts, lithium difluoro-oxalato borate (LiDFOB) is
especially interesting for graphite operation. LiDFOB
electrolytes are conductive at room temperature (ca.
6 mS cm−1) with an anodic stability slightly below
5 V vs. Li/Li+ on particulate carbon black electrodes. In
addition, it allows cycling graphite electrodes with steady
capacity and high coulombic efficiency without any additive.
The testing of graphite electrodes in half-cells is,
however, problematic with SL:DMC mixtures and, by switching
the Li metal counter electrode for LiFePO4, the graphite
electrode achieves better practical performance in terms of
rate capability.},
cin = {IEK-12},
ddc = {620},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000438001800024},
doi = {10.1016/j.jpowsour.2018.05.077},
url = {https://juser.fz-juelich.de/record/863370},
}