TY - JOUR AU - Giese, Sven AU - Neumeier, Steffen AU - Amberger-Matschkal, Doris AU - Bergholz, Jan AU - Vaßen, Robert AU - Göken, Mathias TI - Microtensile creep testing of freestanding MCrAlY bond coats JO - Journal of materials research VL - 34 IS - 15 SN - 2044-5326 CY - Cambridge [u.a.] PB - Cambridge Univ. Press M1 - FZJ-2019-03601 SP - 2643-2652 PY - 2019 AB - Bond coats are essential in gas turbine technology for oxidation protection. Freestanding MCrAlY (M = Ni, Co) bond coats were investigated with respect to their creep strength at elevated temperatures. Three types of MCrAlY, a Ni-based bond coat Amdry 386, a Co-based bond coat Amdry 9954 and Amdry 9954 + 2 wt% Al2O3 (ODS = oxide dispersion strengthened) produced by low pressure plasma spraying, were analyzed. The two phase microstructure of the bond coats consists of a fcc γ-Ni solid solution and a B2 β-NiAl phase. Constant load experiments were performed in a thermomechanical analyzer at temperatures between 900 and 950 °C. Microtensile test specimens with a diameter of 450 µm were produced by a high-precision grinding and polishing process. Creep rupture was mainly due to void nucleation along the β–γ interfaces and grain boundaries. The time to failure is larger in Ni-based Amdry 386 compared to that in Co-based Amdry 9954 due to a higher fraction of the high-strength β-NiAl phase at test temperatures. The addition of ODS-particles in the Co-based bond coat Amdry 9954 resulted in a better creep resistance but lower ductility in comparison to ODS-particle-free Amdry 9954. LB - PUB:(DE-HGF)16 UR - <Go to ISI:>//WOS:000482958400008 DO - DOI:10.1557/jmr.2019.169 UR - https://juser.fz-juelich.de/record/863562 ER -