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| 001 | 864465 | ||
| 005 | 20210130002601.0 | ||
| 024 | 7 | _ | |a 10.1016/j.bmc.2019.04.033 |2 doi |
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| 100 | 1 | _ | |a Mechsner, Bastian |0 P:(DE-Juel1)165893 |b 0 |
| 245 | _ | _ | |a Enantioselective total synthesis of altersolanol A and N |
| 260 | _ | _ | |a Amsterdam [u.a.] |c 2019 |b Elsevier |
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| 520 | _ | _ | |a The development of the first enantioselective total synthesis of altersolanol N is reported. The decisive step of the synthesis is the enantioselective formation of the tetrahydroanthraquinone nucleus by a [4 + 2]-cycloaddition in high yield and with excellent diastereo- and enantioselectivity (>95:5 dr and 95:5 er). In addition, a demanding selective monoacetylation of the OH group at the C-2 position was achieved: an epoxide ring opening with the participation of a neighbouring acetyl group could be established. The route proved to be an efficient alternative to also access enantiomerically pure altersolanol A. |
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| 700 | 1 | _ | |a Böse, Dietrich |0 P:(DE-Juel1)139024 |b 1 |
| 700 | 1 | _ | |a Hogenkamp, Fabian |0 P:(DE-Juel1)169329 |b 2 |
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| 700 | 1 | _ | |a Bochinsky, Kevin |0 P:(DE-Juel1)165763 |b 5 |
| 700 | 1 | _ | |a Frey, Wolfgang |0 P:(DE-HGF)0 |b 6 |
| 700 | 1 | _ | |a Pietruszka, Jörg |0 P:(DE-Juel1)128906 |b 7 |e Corresponding author |
| 773 | _ | _ | |a 10.1016/j.bmc.2019.04.033 |g Vol. 27, no. 13, p. 2991 - 2997 |0 PERI:(DE-600)1501507-5 |n 13 |p 2991 - 2997 |t Bioorganic & medicinal chemistry |v 27 |y 2019 |x 0968-0896 |
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