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| 001 | 865103 | ||
| 005 | 20230426083211.0 | ||
| 024 | 7 | _ | |a 10.1103/PhysRevB.100.014414 |2 doi |
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| 100 | 1 | _ | |a Sazonov, Andrew |0 P:(DE-Juel1)164291 |b 0 |e Corresponding author |u fzj |
| 245 | _ | _ | |a Unambiguous determination of the commensurate antiferromagnetic structure of HoNi 2 B 2 C in the superconducting ground state |
| 260 | _ | _ | |a Woodbury, NY |c 2019 |b Inst. |
| 336 | 7 | _ | |a article |2 DRIVER |
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| 520 | _ | _ | |a Crystal and magnetic structures of the intermetallic HoNi2B2C have been investigated using different single-crystal diffraction techniques at both room and low temperatures (superconducting phase). Combined refinement of the neutron and x-ray diffraction data performed at room temperature shows that the crystal structure of HoNi2B2C is well described in the tetragonal space group I4/mmm, in agreement with the literature. The magnetic ordering at low temperatures is accompanied by a structural phase transition to the orthorhombic space group Fmmm. However, only noncharacteristic orbits are occupied in this space group, and the symmetry reduction is entirely due to a lifting of the symmetry-induced restrictions on the anisotropic displacement parameters. Based on magnetic symmetry analysis, two types of commensurate antiferromagnetic structures with different magnetic space groups (MSGs) are found below TN≈5.2 K: MSG PInnm (Ho spins are along the [100] direction of the parent structure) and MSG CAmca (Ho spins are along [110] of the parent structure). Both models agree well with conventional unpolarized neutron diffraction data at low temperature (2.4 K) with ordered magnetic moments of 9.16(9) μB/Ho3+ atom. Spherical neutron polarimetry, on the other hand, allowed us to unambiguously solve the magnetic structure (MSG CAmca) as well as to determine the population of two types of 90∘ antiferromagnetic domains (0.45/0.55). |
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