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000865916 1001_ $$0P:(DE-Juel1)168112$$aNonemacher, Juliane Franciele$$b0
000865916 245__ $$aMicromechanical Assessment of Al/Y-substituted NASICON Solid Electrolytes
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000865916 520__ $$aAl/Y-substituted NASICON solid electrolytes are promising for novel solid state batteries. The solid solutions Na1+2xAlxYxZr2-2x(PO4)3 (NAYZPx) and Na3+2xAlxYxZr2-2x(SiO4)2(PO4) (NAYZSiPx) that crystallize in this structure are characterized by depth-sensitive indentation technique to determine their micro-mechanical properties. NAYZPx is rhombohedral, whereas NAYZSiPx changes from monoclinic to rhombohedral phase depending on substitutional level and temperature. For rhombohedral NAYZPx elastic moduli are in the range ~72–82 GPa and hardness values are in the range ~4.8–5.8 GPa, whereas for NAYZSiPx the elastic moduli are with the range ~72–88 GPa and hardness ~5.6–7.6 GPa, respectively. The fracture toughness values for both systems, as determined by Vickers indentation, are rather independent of the applied load being with the range 1.30–1.58 MPa m0.5. Cracks typically show a mixed intergranular/transgranular crack mode.
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000865916 7001_ $$0P:(DE-Juel1)165865$$aNaqash, Sahir$$b1$$ufzj
000865916 7001_ $$0P:(DE-Juel1)129667$$aTietz, Frank$$b2$$ufzj
000865916 7001_ $$0P:(DE-Juel1)129755$$aMalzbender, Jürgen$$b3$$eCorresponding author$$ufzj
000865916 773__ $$0PERI:(DE-600)2018052-4$$a10.1016/j.ceramint.2019.07.114$$gVol. 45, no. 17, p. 21308 - 21314$$n17A$$p21308 - 21314$$tCeramics international$$v45$$x0272-8842$$y2019
000865916 8564_ $$uhttps://juser.fz-juelich.de/record/865916/files/11-jun-2019%20%20Micromechanical%20Assessment%20of%20AlY-substituted%20NASICON_vFT_vSN.pdf$$yPublished on 2019-07-09. Available in OpenAccess from 2021-07-09.
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