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@ARTICLE{Kim:867278,
author = {Kim, Un‐Hyuck and Ryu, Hoon‐Hee and Kim, Jae‐Hyung
and Mücke, Robert and Kaghazchi, Payam and Yoon, Chong S.
and Sun, Yang‐Kook},
title = {{M}icrostructure‐{C}ontrolled {N}i‐{R}ich {C}athode
{M}aterial by {M}icroscale {C}ompositional {P}artition for
{N}ext‐{G}eneration {E}lectric {V}ehicles},
journal = {Advanced energy materials},
volume = {9},
number = {15},
issn = {1614-6840},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2019-06036},
pages = {1803902 -},
year = {2019},
abstract = {A multicompositional particulate Li[Ni0.9Co0.05Mn0.05]O2
cathode in which Li[Ni0.94Co0.038Mn0.022]O2 at the particle
center is encapsulated by a 1.5 µm thick concentration
gradient (CG) shell with the outermost surface composition
Li[Ni0.841Co0.077Mn0.082]O2 is synthesized using a
differential coprecipitation process. The microscale
compositional partitioning at the particle level combined
with the radial texturing of the refined primary particles
in the CG shell layer protracts the detrimental H2 → H3
phase transition, causing sharp changes in the unit cell
dimensions. This protraction, confirmed by in situ X‐ray
diffraction and transmission electron microscopy, allows
effective dissipation of the internal strain generated upon
the H2 → H3 phase transition, markedly improving cycling
performance and thermochemical stability as compared to
those of the conventional single‐composition
Li[Ni0.9Co0.05Mn0.05]O2 cathodes. The compositionally
partitioned cathode delivers a discharge capacity of 229 mAh
g−1 and exhibits capacity retention of $88\%$ after 1000
cycles in a pouch‐type full cell (compared to $68\%$ for
the conventional cathode). Thus, the proposed cathode
material provides an opportunity for the rational design and
development of a wide range of multifunctional cathodes,
especially for Ni‐rich Li[NixCoyMn1‐x‐y]O2 cathodes,
by compositionally partitioning the cathode particles and
thus optimizing the microstructural response to the internal
strain produced in the deeply charged state.},
cin = {IEK-1},
ddc = {050},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000465464500010},
doi = {10.1002/aenm.201803902},
url = {https://juser.fz-juelich.de/record/867278},
}