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000867470 1001_ $$0P:(DE-HGF)0$$aKlauke, Karsten$$b0$$eCorresponding author
000867470 245__ $$aSilver, Gold, Palladium, and Platinum N-heterocyclic Carbene Complexes Containing a Selenoether-Functionalized Imidazol-2-ylidene Moiety
000867470 260__ $$aWashington, DC$$bACS Publ.$$c2018
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000867470 520__ $$aThe selenoether-functionalized imidazolium salt N-[(phenylseleno)methylene)]-N′-methylimidazolium chloride (LH+Cl–) was transformed into the metal–carbene complexes [AgCl(L)], [AuCl(L)], [PdCl2(L)], and [PtCl2(L)] by the reaction with Ag2O and an additional transmetalation reaction of [AgCl(L)] with [(THT)AuCl], [(COD)PdCl2], and [(COD)PtCl2], respectively (THT = tetrahydrothiophene, COD = cyclooctadiene). The compound [AuI2Cl(L)] was prepared by oxidation of [AuCl(L)] with elemental iodine. The microwave-assisted decomposition of [PdCl2(L)] in the ionic liquid 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide ([BMIm]NTf2) or in propylene carbonate led to the formation of Pd17Se15 nanoparticles of 51 ± 17 or 26 ± 7 nm diameter, respectively. The decomposition of the platinum complex resulted in either small Pt clusters around 1 nm size from the ionic liquid suspension or Pt nanoparticles of 3 ± 1 nm diameter in propylene carbonate. High-resolution X-ray photoelectron spectroscopy (HR-XPS) and 13C cross-polarization magic-angle spinning (CP MAS) NMR indicated that the surface of Pt clusters and crystalline Pt nanoparticles is formed by an amorphous Pt(II)/Se shell and by carbene ligand residues.
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000867470 7001_ $$0P:(DE-HGF)0$$aGruber, Irina$$b1
000867470 7001_ $$0P:(DE-HGF)0$$aKnedel, Tim-Oliver$$b2
000867470 7001_ $$0P:(DE-HGF)0$$aSchmolke, Laura$$b3
000867470 7001_ $$0P:(DE-Juel1)130525$$aBarthel, Juri$$b4$$ufzj
000867470 7001_ $$0P:(DE-HGF)0$$aBreitzke, Hergen$$b5
000867470 7001_ $$00000-0003-1304-9762$$aBuntkowsky, Gerd$$b6
000867470 7001_ $$00000-0002-6288-9605$$aJaniak, Christoph$$b7
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