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@ARTICLE{Klauke:867470,
      author       = {Klauke, Karsten and Gruber, Irina and Knedel, Tim-Oliver
                      and Schmolke, Laura and Barthel, Juri and Breitzke, Hergen
                      and Buntkowsky, Gerd and Janiak, Christoph},
      title        = {{S}ilver, {G}old, {P}alladium, and {P}latinum
                      {N}-heterocyclic {C}arbene {C}omplexes {C}ontaining a
                      {S}elenoether-{F}unctionalized {I}midazol-2-ylidene
                      {M}oiety},
      journal      = {Organometallics},
      volume       = {37},
      number       = {3},
      issn         = {1520-6041},
      address      = {Washington, DC},
      publisher    = {ACS Publ.},
      reportid     = {FZJ-2019-06109},
      pages        = {298 - 308},
      year         = {2018},
      abstract     = {The selenoether-functionalized imidazolium salt
                      N-[(phenylseleno)methylene)]-N′-methylimidazolium chloride
                      (LH+Cl–) was transformed into the metal–carbene
                      complexes [AgCl(L)], [AuCl(L)], [PdCl2(L)], and [PtCl2(L)]
                      by the reaction with Ag2O and an additional transmetalation
                      reaction of [AgCl(L)] with [(THT)AuCl], [(COD)PdCl2], and
                      [(COD)PtCl2], respectively (THT = tetrahydrothiophene, COD =
                      cyclooctadiene). The compound [AuI2Cl(L)] was prepared by
                      oxidation of [AuCl(L)] with elemental iodine. The
                      microwave-assisted decomposition of [PdCl2(L)] in the ionic
                      liquid 1-butyl-3-methylimidazolium
                      bis(trifluoromethylsulfonyl)imide ([BMIm]NTf2) or in
                      propylene carbonate led to the formation of Pd17Se15
                      nanoparticles of 51 ± 17 or 26 ± 7 nm diameter,
                      respectively. The decomposition of the platinum complex
                      resulted in either small Pt clusters around 1 nm size from
                      the ionic liquid suspension or Pt nanoparticles of 3 ± 1 nm
                      diameter in propylene carbonate. High-resolution X-ray
                      photoelectron spectroscopy (HR-XPS) and 13C
                      cross-polarization magic-angle spinning (CP MAS) NMR
                      indicated that the surface of Pt clusters and crystalline Pt
                      nanoparticles is formed by an amorphous Pt(II)/Se shell and
                      by carbene ligand residues.},
      cin          = {ER-C-2},
      ddc          = {540},
      cid          = {I:(DE-Juel1)ER-C-2-20170209},
      pnm          = {131 - Electrochemical Storage (POF3-131)},
      pid          = {G:(DE-HGF)POF3-131},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000425193000006},
      doi          = {10.1021/acs.organomet.7b00678},
      url          = {https://juser.fz-juelich.de/record/867470},
}