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@ARTICLE{evk:867580,
author = {Ševčík, Radek and Viani, Alberto and Machová, Dita and
Lanzafame, Gabriele and Mancini, Lucia and Appavou,
Marie-Sousai},
title = {{S}ynthetic calcium carbonate improves the effectiveness of
treatments with nanolime to contrast decay in highly porous
limestone},
journal = {Scientific reports},
volume = {9},
number = {1},
issn = {2045-2322},
address = {[London]},
publisher = {Macmillan Publishers Limited, part of Springer Nature},
reportid = {FZJ-2019-06203},
pages = {15278},
year = {2019},
abstract = {Three synthetized polymorphs of calcium carbonate have been
tested in combination with the suspension of nanolime
particles as potential consolidating agents for contrasting
stone decay and overcome some of the limitations of nanolime
agents when applied to substrates with large porosity. The
modifications induced in the pore network of the Maastricht
limestone were analyzed with microscopy and in a
non-invasive fashion with small angle neutron scattering and
synchrotron radiation micro-computed tomography. A reduction
in porosity and pore accessibility at the micrometric scale
was detected with the latter technique, and ascribed to the
improved pore-filling capacity of the consolidation agent
containing CaCO3 particles. These were found to be
effectively bound to the carbonated nanolime, strengthening
the pore-matrix microstructure. Penetration depth and
positive effect on porosity were found to depend on the
particle size and shape. Absence of significant changes in
the fractal nature of the pore surface at the nanoscale, was
interpreted as indication of the negligible contribution of
nanolime-based materials in the consolidation of stones with
large porosity. However, the results indicate that in such
cases, their effectiveness may be enhanced when used in
combination with CaCO3 particles, owing to the synergic
effect of chemical/structural compatibility and particle
size distribution.},
cin = {JCNS-FRM-II / JCNS-1 / MLZ},
ddc = {600},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-1-20110106 / I:(DE-588b)4597118-3},
pnm = {6G4 - Jülich Centre for Neutron Research (JCNS) (POF3-623)
/ 6G15 - FRM II / MLZ (POF3-6G15)},
pid = {G:(DE-HGF)POF3-6G4 / G:(DE-HGF)POF3-6G15},
experiment = {EXP:(DE-MLZ)KWS2-20140101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:31649279},
UT = {WOS:000492141900009},
doi = {10.1038/s41598-019-51836-z},
url = {https://juser.fz-juelich.de/record/867580},
}