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@ARTICLE{GrossBarsnick:867595,
author = {Gross-Barsnick, Sonja-Michaela and Fang, Q. and Batfalsky,
P. and Niewolak, L. and Blum, Ludger and Quadakkers, W. J.},
title = {{P}ost‐test {C}haracterization of {M}etallic {M}aterials
and {A}djacent {C}omponents in an {SOFC} {S}tack {A}fter
34,000 h {O}peration at 700 °{C}},
journal = {Fuel cells},
volume = {19},
number = {1},
issn = {1615-6854},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2019-06216},
pages = {84 - 95},
year = {2019},
abstract = {The present paper describes the electrochemical results and
the post exposure microstructural characterization by means
of SEM/EDS of a four layer SOFC stack after 34,000 h
operation under load at 700 °C, showing low voltage
degradation rate less than $0.3\%$ per 1,000 h. Emphasis was
put on the behavior of the ferritic interconnect steel and
its interaction with glass sealants as well as contacting
and coating materials. The interconnect steel had formed
thin protective chromia scales. Gas distributing steel foils
of 200 µm showed in some locations breakaway type
oxidation. It was related to local overheating caused by
locally occurring combustion of a defective cell. The
interaction of the steel with the glass sealant showed good
adhesion. Interdiffusion at the joint between nickel contact
and steel interconnect at the anode side resulted in minor
oxide formation on the Ni wires and in austenite formation
in the steel without formation of σ‐FeCr formation at the
steel/austenite interface. The steel showed excellent
compatibility with the Manganese‐Cobalt‐Ferrite (MCF)
chromium retention coatings. Chromium enriched phases were
found near the interface between MCF coating and perovskite
contact layer. Excess glass sealing material interacted with
the contact layer without showing obvious detrimental
effects.},
cin = {IEK-2 / IEK-3 / ZEA-1 / IEK-14},
ddc = {620},
cid = {I:(DE-Juel1)IEK-2-20101013 / I:(DE-Juel1)IEK-3-20101013 /
I:(DE-Juel1)ZEA-1-20090406 / I:(DE-Juel1)IEK-14-20191129},
pnm = {113 - Methods and Concepts for Material Development
(POF3-113)},
pid = {G:(DE-HGF)POF3-113},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000458426600010},
doi = {10.1002/fuce.201800050},
url = {https://juser.fz-juelich.de/record/867595},
}