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@ARTICLE{Jung:868386,
author = {Jung, Florian A. and Panteli, Panayiota A. and Ko,
Chia-Hsin and Kang, Jia-Jhen and Barnsley, Lester C. and
Tsitsilianis, Constantinos and Patrickios, Costas S. and
Papadakis, Christine M.},
title = {{S}tructural {P}roperties of {M}icelles {F}ormed by
{T}elechelic {P}entablock {Q}uaterpolymers with
p{H}-{R}esponsive {M}idblocks and {T}hermoresponsive {E}nd
{B}locks in {A}queous {S}olution},
journal = {Macromolecules},
volume = {52},
number = {24},
issn = {1520-5835},
address = {Washington, DC},
publisher = {Soc.},
reportid = {FZJ-2020-00002},
pages = {9746 - 9758},
year = {2019},
abstract = {We investigated the structural properties of dynamic
micelles arising from the self-assembly of the
multiresponsive pentablock quaterpolymer
P(nBuMA8-co-TEGMA8)-b-PDMAEMA50-b-PEG46-b-PDMAEMA50-b-P(nBuMA8-co-TEGMA8)
(nBuMA, TEGMA, DMAEMA, and EG are n-butyl methacrylate,
tri(ethylene glycol) methyl ether methacrylate,
2-(dimethylamino)ethyl methacrylate, and ethylene glycol,
respectively) in aqueous solution using a combination of
scattering methods. In this multisegmented polymer, a
pH-responsive BAB triblock copolymer from the weak cationic
polyelectrolyte PDMAEMA and the hydrophilic PEG is
end-capped by two blocks comprising random sequences of
thermoresponsive TEGMA units and hydrophobic nBuMA units.
Dynamic light scattering revealed the existence of single
micelles and small clusters in dilute aqueous solution. The
hydrodynamic radius of the micelles depends strongly on pH
and temperature. The inner structure of the micelles was
investigated by small-angle X-ray scattering, small-angle
neutron scattering, and static light scattering, and
micelles with a hydrophobic core containing a rather high
fraction of water and a strongly swollen corona were found.
The ratio of loops and dangling ends depends on temperature
and pH.},
cin = {JCNS-FRM-II / MLZ},
ddc = {540},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 / I:(DE-588b)4597118-3},
pnm = {6G4 - Jülich Centre for Neutron Research (JCNS) (POF3-623)
/ 6G15 - FRM II / MLZ (POF3-6G15)},
pid = {G:(DE-HGF)POF3-6G4 / G:(DE-HGF)POF3-6G15},
experiment = {EXP:(DE-MLZ)KWS1-20140101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000505629900035},
doi = {10.1021/acs.macromol.9b01775},
url = {https://juser.fz-juelich.de/record/868386},
}