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000873402 1001_ $$0P:(DE-HGF)0$$aFedeli, Paolo$$b0$$eCorresponding author
000873402 245__ $$aAsymmetric LSCF Membranes Utilizing Commercial Powders
000873402 260__ $$aBasel$$bMDPI$$c2020
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000873402 520__ $$aPowders of constant morphology and quality are indispensable for reproducible ceramic manufacturing. In this study, commercially available powders were characterized regarding their microstructural properties and screened for a reproducible membrane manufacturing process, which was done by sequential tape casting. Basing on this, the slurry composition and ratio of ingredients were systematically varied in order to obtain flat, crack-free green tapes suitable for upscaling of the manufacturing process. Debinding and sintering parameters were adjusted to obtain defect-free membranes with diminished bending. The crucial parameters are the heating ramp, sintering temperature, and dwell time. The microstructure of the asymmetric membranes was investigated, leading to a support porosity of approximately 35% and a membrane layer thickness of around 20 µm. Microstructure and oxygen flux are comparable to asymmetric La0.6Sr0.4Co0.2Fe0.8O3-δ (LSCF) membranes manufactured from custom-made powder, showing an oxygen flux of > 1 mLcm−2min at 900 °C in air/Ar gradient. 
000873402 536__ $$0G:(DE-HGF)POF3-113$$a113 - Methods and Concepts for Material Development (POF3-113)$$cPOF3-113$$fPOF III$$x0
000873402 536__ $$0G:(EU-Grant)608524$$aGREEN-CC - Graded Membranes for Energy Efficient New Generation Carbon Capture Process (608524)$$c608524$$fFP7-ENERGY-2013-1$$x1
000873402 7001_ $$0P:(DE-HGF)0$$aDrago, Francesca$$b1
000873402 7001_ $$0P:(DE-Juel1)129660$$aSchulze-Küppers, Falk$$b2$$ufzj
000873402 7001_ $$0P:(DE-Juel1)129587$$aBaumann, Stefan$$b3$$ufzj
000873402 770__ $$aMembrane Materials for Gas Separation
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