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@ARTICLE{Fedeli:873402,
      author       = {Fedeli, Paolo and Drago, Francesca and Schulze-Küppers,
                      Falk and Baumann, Stefan},
      title        = {{A}symmetric {LSCF} {M}embranes {U}tilizing {C}ommercial
                      {P}owders},
      journal      = {Materials},
      volume       = {13},
      number       = {3},
      issn         = {1996-1944},
      address      = {Basel},
      publisher    = {MDPI},
      reportid     = {FZJ-2020-00712},
      pages        = {614},
      year         = {2020},
      abstract     = {Powders of constant morphology and quality are
                      indispensable for reproducible ceramic manufacturing. In
                      this study, commercially available powders were
                      characterized regarding their microstructural properties and
                      screened for a reproducible membrane manufacturing process,
                      which was done by sequential tape casting. Basing on this,
                      the slurry composition and ratio of ingredients were
                      systematically varied in order to obtain flat, crack-free
                      green tapes suitable for upscaling of the manufacturing
                      process. Debinding and sintering parameters were adjusted to
                      obtain defect-free membranes with diminished bending. The
                      crucial parameters are the heating ramp, sintering
                      temperature, and dwell time. The microstructure of the
                      asymmetric membranes was investigated, leading to a support
                      porosity of approximately $35\%$ and a membrane layer
                      thickness of around 20 µm. Microstructure and oxygen flux
                      are comparable to asymmetric La0.6Sr0.4Co0.2Fe0.8O3-δ
                      (LSCF) membranes manufactured from custom-made powder,
                      showing an oxygen flux of > 1 mLcm−2min at 900 °C in
                      air/Ar gradient.},
      cin          = {IEK-1},
      ddc          = {600},
      cid          = {I:(DE-Juel1)IEK-1-20101013},
      pnm          = {113 - Methods and Concepts for Material Development
                      (POF3-113) / GREEN-CC - Graded Membranes for Energy
                      Efficient New Generation Carbon Capture Process (608524)},
      pid          = {G:(DE-HGF)POF3-113 / G:(EU-Grant)608524},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {pmid:32019115},
      UT           = {WOS:000515503100121},
      doi          = {10.3390/ma13030614},
      url          = {https://juser.fz-juelich.de/record/873402},
}