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| 001 | 873402 | ||
| 005 | 20240711085629.0 | ||
| 024 | 7 | _ | |a 10.3390/ma13030614 |2 doi |
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| 082 | _ | _ | |a 600 |
| 100 | 1 | _ | |a Fedeli, Paolo |0 P:(DE-HGF)0 |b 0 |e Corresponding author |
| 245 | _ | _ | |a Asymmetric LSCF Membranes Utilizing Commercial Powders |
| 260 | _ | _ | |a Basel |c 2020 |b MDPI |
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| 336 | 7 | _ | |a Journal Article |0 0 |2 EndNote |
| 520 | _ | _ | |a Powders of constant morphology and quality are indispensable for reproducible ceramic manufacturing. In this study, commercially available powders were characterized regarding their microstructural properties and screened for a reproducible membrane manufacturing process, which was done by sequential tape casting. Basing on this, the slurry composition and ratio of ingredients were systematically varied in order to obtain flat, crack-free green tapes suitable for upscaling of the manufacturing process. Debinding and sintering parameters were adjusted to obtain defect-free membranes with diminished bending. The crucial parameters are the heating ramp, sintering temperature, and dwell time. The microstructure of the asymmetric membranes was investigated, leading to a support porosity of approximately 35% and a membrane layer thickness of around 20 µm. Microstructure and oxygen flux are comparable to asymmetric La0.6Sr0.4Co0.2Fe0.8O3-δ (LSCF) membranes manufactured from custom-made powder, showing an oxygen flux of > 1 mLcm−2min at 900 °C in air/Ar gradient. |
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| 536 | _ | _ | |a GREEN-CC - Graded Membranes for Energy Efficient New Generation Carbon Capture Process (608524) |0 G:(EU-Grant)608524 |c 608524 |f FP7-ENERGY-2013-1 |x 1 |
| 700 | 1 | _ | |a Drago, Francesca |0 P:(DE-HGF)0 |b 1 |
| 700 | 1 | _ | |a Schulze-Küppers, Falk |0 P:(DE-Juel1)129660 |b 2 |u fzj |
| 700 | 1 | _ | |a Baumann, Stefan |0 P:(DE-Juel1)129587 |b 3 |u fzj |
| 770 | _ | _ | |a Membrane Materials for Gas Separation |
| 773 | _ | _ | |a 10.3390/ma13030614 |0 PERI:(DE-600)2487261-1 |n 3 |p 614 |t Materials |v 13 |y 2020 |x 1996-1944 |
| 856 | 4 | _ | |y OpenAccess |u https://juser.fz-juelich.de/record/873402/files/Fedeli20%20-%20Asymmetric%20LSCF%20membranes%20utilizing%20commercial%20powders.pdf |
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