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@ARTICLE{Schupsky:875297,
      author       = {Schupsky, Jan Peter and Wu, Guixuan and Guo, Muxing and
                      Müller, Michael},
      title        = {{C}rystallisation characteristics and crystal phase
                      quantification of a synthetic lignite gasifier slag system},
      journal      = {Fuel processing technology},
      volume       = {201},
      issn         = {0378-3820},
      address      = {New York, NY [u.a.]},
      publisher    = {Science Direct},
      reportid     = {FZJ-2020-01928},
      pages        = {106345 -},
      year         = {2020},
      abstract     = {The scope of this study is to investigate the
                      crystallisation phenomenon of a synthetic
                      SiO2-Al2O3-CaO-Fe2O3-MgO slag system. Firstly, the
                      crystallised phases were predicted by thermodynamic
                      equilibrium calculations. Subsequently, quenching
                      experiments and confocal laser scanning microscope (CLSM)
                      investigations were performed to validate the
                      crystallisation characteristics of the synthetic slag
                      system. Crystallisation kinetics was examined by isothermal
                      quenching and continuous cooling CLSM experiments. The
                      generated samples were analysed by microscopy, XRD, and SEM
                      to determine the crystallised phases by their structure and
                      chemical composition. A detailed insight of the evolution of
                      crystal morphology growth was given. The shape of the two
                      dominant phases: melilite and olivine were described and
                      three-dimensional morphologies were defined for both phases.
                      Additionally, the morphologies were quantified by length and
                      aspect ratio measurements of individual crystals. The
                      morphological information of the olivine and melilite phase,
                      provided in this study, can be used as datasets for a
                      viscosity model for partially crystallised slags. A
                      conceptual viscosity model to be implemented in the next
                      paper of this series, using specialised crystal morphology
                      datasets, can serve a major contribution to forecast slag
                      behaviour and to support the stability of industrial
                      gasifier operation.},
      cin          = {IEK-2},
      ddc          = {660},
      cid          = {I:(DE-Juel1)IEK-2-20101013},
      pnm          = {113 - Methods and Concepts for Material Development
                      (POF3-113)},
      pid          = {G:(DE-HGF)POF3-113},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000521519800016},
      doi          = {10.1016/j.fuproc.2020.106345},
      url          = {https://juser.fz-juelich.de/record/875297},
}