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@ARTICLE{Ivanova:877279,
author = {Ivanova, Alesja and Frka-Petesic, Bruno and Paul, Andrej
and Wagner, Thorsten and Jumabekov, Askhat N. and Vilk, Yury
and Weber, Johannes and Schmedt auf der Günne, Jörn and
Vignolini, Silvia and Tiemann, Michael and
Fattakhova-Rohlfing, Dina and Bein, Thomas},
title = {{C}ellulose {N}anocrystal-{T}emplated {T}in {D}ioxide
{T}hin {F}ilms for {G}as {S}ensing},
journal = {ACS applied materials $\&$ interfaces},
volume = {12},
number = {11},
issn = {1944-8252},
address = {Washington, DC},
publisher = {Soc.},
reportid = {FZJ-2020-02102},
pages = {12639 - 12647},
year = {2020},
note = {Kein Post-print vorhanden!},
abstract = {Porous tin dioxide is an important low-cost semiconductor
applied in electronics, gas sensors, and biosensors. Here,
we present a versatile template-assisted synthesis of
nanostructured tin dioxide thin films using cellulose
nanocrystals (CNCs). We demonstrate that the structural
features of CNC-templated tin dioxide films strongly depend
on the precursor composition. The precursor properties were
studied by using low-temperature nuclear magnetic resonance
spectroscopy of tin tetrachloride in solution. We
demonstrate that it is possible to optimize the precursor
conditions to obtain homogeneous precursor mixtures and
therefore highly porous thin films with pore dimensions in
the range of 10–20 nm (ABET = 46–64 m2 g–1, measured
on powder). Finally, by exploiting the high surface area of
the material, we developed a resistive gas sensor based on
CNC-templated tin dioxide. The sensor shows high sensitivity
to carbon monoxide (CO) in ppm concentrations and low
cross-sensitivity to humidity. Most importantly, the sensing
kinetics are remarkably fast; both the response to the
analyte gas and the signal decay after gas exposure occur
within a few seconds, faster than in standard SnO2-based CO
sensors. This is attributed to the high gas accessibility of
the very thin porous film.},
cin = {IEK-1},
ddc = {600},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
pubmed = {31898457},
UT = {WOS:000526543400026},
doi = {10.1021/acsami.9b11891},
url = {https://juser.fz-juelich.de/record/877279},
}