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@ARTICLE{Pipich:877601,
author = {Pipich, Vitaliy and Schwahn, Dietmar},
title = {{P}olymorphic phase transition in liquid and supercritical
carbon dioxide},
journal = {Scientific reports},
volume = {10},
number = {1},
issn = {2045-2322},
address = {[London]},
publisher = {Macmillan Publishers Limited, part of Springer Nature},
reportid = {FZJ-2020-02316},
pages = {11861},
year = {2020},
abstract = {We present experiments on molecular density fluctuations in
liquid and supercritical (SC) CO2 using small-angle neutron
scattering. Thermal density fluctuations in SC-CO2 determine
susceptibility and correlation length identifying the Widom
line at their maxima. Droplet formation occurs at the
gas–liquid line and between 20 and 60 bar above the Widom
line, the corresponding borderline identified as the Frenkel
line. The droplets start to form spheres of constant radius
of ≈ 45 Å and transform into rods and globules at higher
pressure. Droplet formation represents a liquid–liquid
(polymorphic) phase transition of the same composition but
different density, whose difference defines its order
parameter. Polymorphism in CO2 is a new observation
stimulating interesting discussions on the topics of
gas-like to liquid-like transition in SC fluids and
polymorphism since CO2 represents a “simple” van der
Waals liquid in contrast to water, which is the most widely
studied liquid showing polymorphism in its supercooled
state.},
cin = {JCNS-1 / JCNS-4 / JCNS-FRM-II / MLZ},
ddc = {600},
cid = {I:(DE-Juel1)JCNS-1-20110106 / I:(DE-Juel1)JCNS-4-20201012 /
I:(DE-Juel1)JCNS-FRM-II-20110218 / I:(DE-588b)4597118-3},
pnm = {6G4 - Jülich Centre for Neutron Research (JCNS) (POF3-623)
/ 6215 - Soft Matter, Health and Life Sciences (POF3-621) /
6G15 - FRM II / MLZ (POF3-6G15)},
pid = {G:(DE-HGF)POF3-6G4 / G:(DE-HGF)POF3-6215 /
G:(DE-HGF)POF3-6G15},
experiment = {EXP:(DE-MLZ)KWS1-20140101},
typ = {PUB:(DE-HGF)16},
pubmed = {32681012},
UT = {WOS:000549998300003},
doi = {10.1038/s41598-020-68451-y},
url = {https://juser.fz-juelich.de/record/877601},
}