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@ARTICLE{Celentano:877980,
author = {Celentano, G. and Rizzo, F. and Augieri, A. and Mancini, A.
and Pinto, V. and Rufoloni, A. and Vannozzi, A. and
MacManus-Driscoll, J. L. and Feighan, J. and Kursumovic, A.
and Meledin, A. and Mayer, J. and Van Tendeloo, G.},
title = {{YB}a 2 {C}u 3 {O} 7−x films with {B}a 2
{Y}({N}b,{T}a){O} 6 nanoinclusions for high-field
applications},
journal = {Superconductor science and technology},
volume = {33},
number = {4},
issn = {1361-6668},
address = {Bristol},
publisher = {IOP Publ.},
reportid = {FZJ-2020-02554},
pages = {044010 -},
year = {2020},
abstract = {The structural and transport properties of YBa2Cu3O7−x
films grown by pulsed laser deposition with mixed 2.5
$mol\%$ Ba2YTaO6 (BYTO) and 2.5 $mol\%$ Ba2YNbO6 (BYNO)
double-perovskite secondary phases are investigated in an
extended film growth rate, R = 0.02–1.8 nm s−1. The
effect of R on the film microstructure analyzed by TEM
techniques shows an evolution from sparse and straight to
denser, thinner and splayed continuous columns, with mixed
BYNO + BYTO (BYNTO) composition, as R increases from 0.02 nm
s−1 to 1.2 nm s−1. This microstructure results in very
efficient flux pinning at 77 K, leading to a remarkable
improvement in the critical current density (Jc) behaviour,
with the maximum pinning force density Fp(Max) = 13.5 GN
m−3 and the irreversibility field in excess of 11 T. In
this range, the magnetic field values at which the Fp is
maximized varies from 1 T to 5 T, being related to the BYNTO
columnar density. The film deposited when R = 0.3 nm s−1
exhibits the best performances over the whole temperature
and magnetic field ranges, achieving Fp(Max) = 900 GN m−3
at 10 K and 12 T. At higher rates, R > 1.2 nm s−1, BYNTO
columns show a meandering nature and are prone to form short
nanorods. In addition, in the YBCO film matrix a more
disordered structure with a high density of short stacking
faults is observed. From the analysis of the Fp(H, T) curves
it emerges that in films deposited at the high R limit, the
vortex pinning is no longer dominated by BYNTO columnar
defects, but by a new mechanism showing the typical
temperature scaling law. Even though this microstructure
produces a limited improvement at 77 K, it exhibits a strong
Jc improvement at lower temperature with Fp = 700 GN m−3
at 10 K, 12 T and 900 GN m−3 at 4.2 K, 18 T.},
cin = {ER-C-2},
ddc = {530},
cid = {I:(DE-Juel1)ER-C-2-20170209},
pnm = {143 - Controlling Configuration-Based Phenomena (POF3-143)
/ ESTEEM3 - Enabling Science and Technology through European
Electron Microscopy (823717)},
pid = {G:(DE-HGF)POF3-143 / G:(EU-Grant)823717},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000525650500001},
doi = {10.1088/1361-6668/ab6ee5},
url = {https://juser.fz-juelich.de/record/877980},
}