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000878151 1001_ $$00000-0002-6277-1252$$aScarfiello, Riccardo$$b0$$eCorresponding author
000878151 245__ $$aMechanistic insight into the formation of colloidal WS 2 nanoflakes in hot alkylamine media
000878151 260__ $$aCambridge$$bRoyal Society of Chemistry$$c2019
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000878151 520__ $$aDeveloping convenient and reliable synthetic methodologies for solution processable 2D layered ultrathin nanostructures with lateral size control is one of the major challenges for practical applications. In this study, a rational understanding a long-chain amphiphilic surfactant assisted non-hydrolytic synthesis that is able to generate dimension-controllable 2D-WS2 nanocrystal flakes in a single-step protocol is proposed. The evolution of the starting soft organic–inorganic lamellar template into ultrathin few-layer 2D-WS2 nanostructures with lateral size modulation over a range between 3 and 30 nm is monitored. The initial formation of WS2 nanoseeds occurs in a self-assembled sacrificial precursor source, acting as a template, where larger two-dimensional nanostructures can grow without undergoing significant thickness variation. Overall, the chemical nature and steric hindrance of the alkylamines are essential to modulate the reactivity of such WS2 nanoclusters, which correlate with the lateral size of the resulting nanoflakes
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000878151 7001_ $$0P:(DE-HGF)0$$aAltamura, Davide$$b2
000878151 7001_ $$00000-0002-7373-1627$$aMasi, Sofia$$b3
000878151 7001_ $$0P:(DE-HGF)0$$aNobile, Concetta$$b4
000878151 7001_ $$00000-0001-6916-321X$$aBalzano, Federica$$b5
000878151 7001_ $$00000-0003-0983-2885$$aGiannini, Cinzia$$b6
000878151 7001_ $$0P:(DE-HGF)0$$aGrillo, Vincenzo$$b7
000878151 7001_ $$0P:(DE-Juel1)157886$$aTavabi, Amir H.$$b8$$ufzj
000878151 7001_ $$0P:(DE-Juel1)144121$$aDunin-Borkowski, Rafal E.$$b9$$ufzj
000878151 7001_ $$00000-0001-6735-2711$$aUccello-Barretta, Gloria$$b10
000878151 7001_ $$00000-0001-8037-6937$$aCozzoli, P. Davide$$b11
000878151 7001_ $$00000-0002-4570-7777$$aRizzo, Aurora$$b12
000878151 773__ $$0PERI:(DE-600)2942874-9$$a10.1039/C9NA00279K$$gVol. 1, no. 7, p. 2772 - 2782$$n7$$p2772 - 2782$$tNanoscale advances$$v1$$x2516-0230$$y2019
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