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000878512 1001_ $$0P:(DE-Juel1)176281$$aCraig, Austin$$b0
000878512 245__ $$aPreparation of labeled aromatic amino acids via late-stage 18 F-fluorination of chiral nickel and copper complexes
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000878512 520__ $$aA general protocol for the preparation of 18F-labeled AAAs and α-methyl-AAAs applying alcohol-enhanced Cu-mediated radiofluorination of Bpin-substituted chiral complexes using Ni/Cu-BPX templates as double protecting groups is reported. The chiral auxiliaries are easily accessible from commercially available starting materials in a few synthetic steps. The versatility of the method was demonstrated by the high-yielding preparation of a series of [18F]F-AAAs and the successful implementation of the protocol into automated radiosynthesis modules.
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000878512 7001_ $$0P:(DE-Juel1)178654$$aKolks, Niklas$$b1$$ufzj
000878512 7001_ $$0P:(DE-Juel1)176705$$aUrusova, Elizaveta$$b2$$ufzj
000878512 7001_ $$0P:(DE-Juel1)166483$$aZischler, Johannes$$b3
000878512 7001_ $$0P:(DE-Juel1)131826$$aBrugger, Melanie$$b4$$ufzj
000878512 7001_ $$0P:(DE-Juel1)180330$$aEndepols, Heike$$b5
000878512 7001_ $$0P:(DE-Juel1)166419$$aNeumaier, Bernd$$b6$$eCorresponding author
000878512 7001_ $$0P:(DE-Juel1)176188$$aZlatopolskiy, Boris D.$$b7
000878512 773__ $$0PERI:(DE-600)1472881-3$$a10.1039/D0CC02223C$$gVol. 56, no. 66, p. 9505 - 9508$$n66$$p9505 - 9508$$tChemical communications$$v56$$x1364-548X$$y2020
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