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001     878579
005     20240711085706.0
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100 1 _ |0 P:(DE-Juel1)171462
|a Dash, Apurv
|b 0
|e Corresponding author
245 _ _ |a Molten salt shielded synthesis of oxidation prone materials in air
260 _ _ |a Basingstoke
|b Nature Publishing Group
|c 2019
336 7 _ |0 PUB:(DE-HGF)25
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|a Preprint
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|s 1599468619_14754
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336 7 _ |0 28
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336 7 _ |2 BibTeX
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336 7 _ |2 DataCite
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520 _ _ |a To prevent spontaneous oxidation during the high-temperature synthesis of non-oxide ceramics, an inert atmosphere is conventionally required1,2. This, however, results in high energy demand and high production costs. Here, we present a process for the synthesis and consolidation of oxidation-prone materials, the ‘molten salt shielded synthesis/sintering’ process (MS3), which uses molten salts as a reaction medium and also to protect the ceramic powders from oxidation during high-temperature processing in air. Synthesis temperatures are also reduced, and the final product is a highly pure, fine and loose powder that does not require additional milling steps. MS3 has been used for the synthesis of different ternary transition metal compounds (MAX phases, such as Ti3SiC23, Ti2AlN4, MoAlB5), binary carbides (TiC) and for the sintering of titanium. The availability of high-quality powders, combined with energy and cost savings, may remove one of the bottlenecks for the industrial application of these materials.
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700 1 _ |0 P:(DE-Juel1)129670
|a Vaßen, Robert
|b 1
700 1 _ |0 P:(DE-Juel1)161591
|a Guillon, Olivier
|b 2
700 1 _ |0 P:(DE-Juel1)162271
|a Gonzalez-Julian, Jesus
|b 3
773 _ _ |0 PERI:(DE-600)2088679-2
|n 5
|p 465 - 470
|t Nature materials
|v 18
|x 1476-4660
|y 2019
856 4 _ |u https://juser.fz-juelich.de/record/878579/files/Preprint.pdf
|y OpenAccess
856 4 _ |u https://juser.fz-juelich.de/record/878579/files/Preprint.pdf?subformat=pdfa
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|l Energieeffizienz, Materialien und Ressourcen
|v Methods and Concepts for Material Development
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914 1 _ |y 2020
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