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@ARTICLE{Schwab:878682,
author = {Schwab, C. and Höweling, A. and Windmüller, Anna and
Gonzalez-Julian, J. and Möller, Sören and Binder, J. R.
and Uhlenbruck, S. and Guillon, O. and Martin, M.},
title = {{B}ulk and grain boundary {L}i-diffusion in dense
{L}i{M}n2{O}4 pellets by means of isotope exchange and
{T}o{F}-{SIMS} analysis},
journal = {Physical chemistry, chemical physics},
volume = {21},
number = {47},
issn = {1463-9084},
address = {Cambridge},
publisher = {RSC Publ.},
reportid = {FZJ-2020-03000},
pages = {26066 - 26076},
year = {2019},
abstract = {Lithium diffusion in LiMn2O4 pellets is studied by means of
isotope exchange and Time-of-Flight Secondary Ion Mass
Spectrometry (ToF-SIMS). A 6Li-enriched film deposited by
Pulsed Laser Deposition (PLD) on a dense LiMn2O4 pellet with
natural abundance of lithium isotopes is used to study the
tracer diffusion of lithium. The measured profiles are
analyzed by numerical models describing the 6Li tracer
diffusion from the film into the pellet. Experiments in the
Harrison type B regime of diffusion kinetics allow for the
distinction and simultaneous determination of bulk and grain
boundary diffusion coefficients. Changing the experimental
conditions to reach Harrison type A behavior yields
effective diffusion coefficients for lithium tracer
diffusion in LiMn2O4. Activation energies for bulk and grain
boundary diffusion were obtained from experiments at
different temperatures. Our values are critically compared
to previous studies.},
cin = {IEK-1 / IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-1-20101013 / I:(DE-Juel1)IEK-12-20141217},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:31746869},
UT = {WOS:000501356000011},
doi = {10.1039/C9CP05128G},
url = {https://juser.fz-juelich.de/record/878682},
}