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@INPROCEEDINGS{Mishra:885552,
author = {Mishra, Tarini Prasad and Ingraci Neto, R. R. and Raj, R.
and Guillon, O. and Bram, M.},
title = {{C}urrent rate controlled flash sintering of {G}adolinium
doped ceria with tailored microstructure},
reportid = {FZJ-2020-03923},
year = {2020},
abstract = {Recently, current rate controlled flash sintering was
introduced as alternative to established voltage-to-current
control mode. Due to its mixed ionic and electronic
conductivity, Gadolinium doped ceria (GDC) is a good
candidate for demonstrating the potential of this novel
operation mode. Therefore, dog bone shaped GDC samples were
placed in a tube furnace and heated to 680°C. Current rate
was linearly increased at well-defined rates in the range
between 20 and 1000 mA min-1 to a maximum current density of
200 mA min-1. The electric field is self-generated by the
resistivity of the sample. Drop of electric field indicated
the on-set of the flash event. Microstructural
investigations reveal that current rate controlled flash
sintering increases the homogeneity of the grain size
distribution and enables to tailor the grain size.
Furthermore, it is expected that this novel operation mode
ease scaling up of flash sintering technique by reducing the
risk of hot spot formation.},
month = {Sep},
date = {2020-09-22},
organization = {MSE - Materials Science and
Engineering, online (Germany), 22 Sep
2020 - 25 Sep 2020},
subtyp = {Other},
cin = {IEK-1},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {899 - ohne Topic (POF3-899)},
pid = {G:(DE-HGF)POF3-899},
typ = {PUB:(DE-HGF)6},
url = {https://juser.fz-juelich.de/record/885552},
}