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@ARTICLE{Basak:885576,
author = {Basak, Shibabrata and Baaij, Siemen and Ganapathy, Swapna
and George, Chandramohan and Tempel, Hermann and Kungl, Hans
and Kelder, Erik M. and Zandbergen, Henny W. and Wagemaker,
Marnix and Eichel, Rüdiger-A.},
title = {{A}ccessing {L}ithium–{O}xygen {B}attery {D}ischarge
{P}roducts in {T}heir {N}ative {E}nvironments via
{T}ransmission {E}lectron {M}icroscopy {G}rid {E}lectrode},
journal = {ACS applied energy materials},
volume = {3},
number = {10},
issn = {2574-0962},
address = {Washington, DC},
publisher = {ACS Publications},
reportid = {FZJ-2020-03940},
pages = {9509-9515},
year = {2020},
abstract = {High-fidelity and facile ex situ transmission electron
microscopy (TEM) characterization of lithium–oxygen
(Li–O2) batteries is still limited by challenges in
preserving the native environment of Li–O2 discharge
products. The extreme reactivity and moisture sensitivity of
the discharge products means that they are quickly altered
during sample retrieval from cycled batteries and transfer
for TEM analysis, resulting in loss of original information.
We here demonstrate that by using a TEM specimen grid
directly in Li–O2 batteries as both support electrode and
sample collector overlaid on a standard oxygen diffusion
electrode, discharge products that are formed on the grid
can be kept pristine.},
cin = {IEK-9},
ddc = {540},
cid = {I:(DE-Juel1)IEK-9-20110218},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000586710300005},
doi = {10.1021/acsaem.0c01803},
url = {https://juser.fz-juelich.de/record/885576},
}