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000885682 1001_ $$0P:(DE-HGF)0$$aÜberrück, Till$$b0
000885682 245__ $$aA compact X-Band ODNP spectrometer towards hyperpolarized 1H spectroscopy
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000885682 520__ $$aThe demand for compact benchtop NMR systems that can resolve chemical shift differences in the ppm to sub-ppm range is growing. However due to material and size restrictions these magnets are limited in field strength and thus in signal intensity and quality. The implementation of standard hyperpolarization techniques is a next step in an effort to boost the signal. Here we present a compact Overhauser Dynamic Nuclear Polarization (ODNP) setup with a permanent magnet that can resolve 1H chemical shift differences in the ppm range. The assembly of the setup and its components are described in detail, and the functionality of the setup is demonstrated experimentally with ODNP enhanced relaxation measurements yielding a maximal enhancement of −140 for an aqueous 4-hydroxy-TEMPO solution. Additionally, 1H spectroscopic resolution and significant enhancements are demonstrated on acetic acid as a solvent.
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000885682 7001_ $$0P:(DE-HGF)0$$aAdams, Michael$$b1
000885682 7001_ $$0P:(DE-Juel1)162401$$aGranwehr, Josef$$b2
000885682 7001_ $$0P:(DE-HGF)0$$aBlümich, Bernhard$$b3$$eCorresponding author
000885682 773__ $$0PERI:(DE-600)1469665-4$$a10.1016/j.jmr.2020.106724$$gVol. 314, p. 106724 -$$p106724 -$$tJournal of magnetic resonance$$v314$$x1090-7807$$y2020
000885682 8564_ $$uhttps://juser.fz-juelich.de/record/885682/files/ODNP_hardware_revision_BB_2.pdf$$yPublished on 2020-04-02. Available in OpenAccess from 2021-04-02.
000885682 8564_ $$uhttps://juser.fz-juelich.de/record/885682/files/ueberrueck_JMR_314_106724_SI.pdf$$yPublished on 2020-04-02. Available in OpenAccess from 2021-04-02.
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