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@ARTICLE{Beker:885727,
      author       = {Beker, Anne France and Sun, Hongyu and Lemang, Mathilde and
                      van Omme, Johannes Tijn and Spruit, Ronald and Bremmer, G.
                      M. and Basak, Shibabrata and Perez Garza, Hector Hugo},
      title        = {{I}n {S}itu {E}lectrochemistry inside the {TEM} with
                      {C}ontrolled {M}ass {T}ransport},
      journal      = {Nanoscale},
      volume       = {12},
      number       = {43},
      issn         = {2040-3372},
      address      = {Cambridge},
      publisher    = {RSC Publ.},
      reportid     = {FZJ-2020-04039},
      pages        = {22192-22201},
      year         = {2020},
      abstract     = {The field of electrochemistry promises solutions for the
                      future energy crisis and environmental deterioration by
                      developing optimized batteries, fuel-cells and catalysts.
                      Combined with in situ transmission electron microscopy
                      (TEM), it can reveal functional and structural changes. A
                      drawback of this relatively young field is lack of
                      reproducibility in controlling the liquid environment while
                      retaining the imaging and analytical capabilities. Here, a
                      platform for in situ electrochemical studies inside a TEM
                      with a pressure-driven flow is presented, with the
                      capability to control the flow direction and to ensure the
                      liquid will always pass through the region of interest. As a
                      result, the system offers the opportunity to define the mass
                      transport and control the electric potential, giving access
                      to the full kinetics of the redox reaction. In order to show
                      the benefits of the system, copper dendrites are
                      electrodeposited and show reliable electric potential
                      control. Next, their morphology is changed by tuning the
                      mass transport conditions. Finally, at a liquid thickness of
                      approximately 100 nm, the diffraction pattern revealed the
                      〈1,1,1〉 planes of the copper crystals, indicating an
                      atomic resolution down to 2.15 Å. Such control of the
                      liquid thickness enabled elemental mapping, allowing us to
                      distinguish the spatial distribution of different elements
                      in liquid.},
      cin          = {IEK-9},
      ddc          = {600},
      cid          = {I:(DE-Juel1)IEK-9-20110218},
      pnm          = {131 - Electrochemical Storage (POF3-131)},
      pid          = {G:(DE-HGF)POF3-131},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {33136106},
      UT           = {WOS:000589051700022},
      doi          = {10.1039/D0NR04961A},
      url          = {https://juser.fz-juelich.de/record/885727},
}