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@ARTICLE{Falkenstein:885961,
author = {Falkenstein, Andreas and De Souza, Roger A. and Meulenberg,
Wilhelm Albert and Martin, Manfred},
title = {{A} quantitative analysis of two-fold electrical
conductivity relaxation behaviour in mixed
proton–oxide-ion–electron conductors upon hydration},
journal = {Physical chemistry, chemical physics},
volume = {22},
number = {43},
issn = {1463-9084},
address = {Cambridge},
publisher = {RSC Publ.},
reportid = {FZJ-2020-04192},
pages = {25032-25041},
year = {2020},
abstract = {Electrical conductivity relaxation experiments on oxides
with three mobile charge carriers, H+, O2− and e−, yield
in (de-)hydration experiments kinetic parameters (diffusion
coefficients and surface reaction constants). In addition,
three amplitude factors are obtained, but they have not been
given further consideration because quantitative expressions
for their forms are lacking. In this study, the forms of the
amplitude factors are derived for a diffusion-limited and a
surface-reaction-limited case and a mixed case. In order to
demonstrate the benefits of the approach, the electrical
conductivity relaxation behaviour of lanthanum tungstate
(La5.4WO11.1, LaWO54) was investigated experimentally over
the temperature range 923 ≤ T/K ≤ 1223. A switch from
two-fold non-monotonic relaxation behaviour at high
temperatures to two-fold monotonic behaviour at low
temperatures upon hydration was observed. The switch in sign
of the fast kinetics' amplitude factor can be assigned to
the electrochemical mobility of protons surpassing the
electron–hole mobility with decreasing temperature.},
cin = {IEK-1},
ddc = {540},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {113 - Methods and Concepts for Material Development
(POF3-113)},
pid = {G:(DE-HGF)POF3-113},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:33112301},
UT = {WOS:000588601200015},
doi = {10.1039/D0CP03264F},
url = {https://juser.fz-juelich.de/record/885961},
}