Hauptseite > Publikationsdatenbank > A Novel Approach for the Quantification of Different Inorganic and Organic Phosphorus Compounds in Environmental Samples by P L 2,3 -Edge X-ray Absorption Near-Edge Structure (XANES) Spectroscopy > print

001     887795
005     20210426112046.0
024 7 _ |a 10.1021/acs.est.9b07018
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024 7 _ |a 1520-5851
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037 _ _ |a FZJ-2020-04425
082 _ _ |a 333.7
100 1 _ |a Colocho Hurtarte, Luis Carlos
|0 0000-0002-1791-2298
|b 0
|e Corresponding author
245 _ _ |a A Novel Approach for the Quantification of Different Inorganic and Organic Phosphorus Compounds in Environmental Samples by P L 2,3 -Edge X-ray Absorption Near-Edge Structure (XANES) Spectroscopy
260 _ _ |a Columbus, Ohio
|c 2020
|b American Chemical Society
336 7 _ |a article
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520 _ _ |a Phosphorus (P) is an essential element for life on Earth, with an important and oftentimes unaccounted organic biogeochemical component. Current methods for the quantification of different organic P compounds in environmental samples (e.g., soils, sediments) are based on extraction techniques and often associated with incomplete P recovery or sample changes. In this study, we present a protocol for the quantification of different organic and inorganic P species in soils using synchrotron-based X-ray absorption near-edge structure (XANES) spectroscopy at the P L2,3-edge. Its accuracy and precision was evaluated by analyzing 40 standard mixtures composed of seven different inorganic and organic P compounds (with a mean of R2 = 0.85). In addition, we quantified the P species of two soils and two agro-industrial byproducts using P L2,3-edge XANES spectroscopy and the results were compared with those obtained by P K-edge XANES or 31P NMR spectroscopy. Using the P L2,3-edge, we identified different organic P species, including those not identified by the common P K-edge XANES. However, there is a consistent underestimation of organic polyphosphates. Overall, the application of P L2,3-edge XANES provides a higher level of information than by P K-edge XANES, although the ubiquitous use of this novel methodology is still limited to samples with a phosphorus content above 3 mg g–1.
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700 1 _ |a Santana Amorim, Helen Carla
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700 1 _ |a Kruse, Jens
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700 1 _ |a Criginski Cezar, Julio
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700 1 _ |a Klysubun, Wantana
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700 1 _ |a Prietzel, Jörg
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773 _ _ |a 10.1021/acs.est.9b07018
|g Vol. 54, no. 5, p. 2812 - 2820
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|t Environmental science & technology
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|y 2020
|x 1520-5851
856 4 _ |y Published on 2020-02-18. Available in OpenAccess from 2021-02-18.
|u https://juser.fz-juelich.de/record/887795/files/Manuscript%20P%20L%20edge_Aceptedchanges.docx
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