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@ARTICLE{Rheinheimer:887826,
author = {Rheinheimer, Wolfgang and Phuah, Xin Li and Wang, Han and
Lemke, Fabian and Hoffmann, Michael J. and Wang, Haiyan},
title = {{T}he role of point defects and defect gradients in flash
sintering of perovskite oxides},
journal = {Acta materialia},
volume = {165},
issn = {1359-6454},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2020-04452},
pages = {398 - 408},
year = {2019},
abstract = {The present study investigates the impact of point defects
and their redistribution on the flash sintering process.
Strontium titanate was chosen as a model system for the
group of perovskite ceramics. The characteristics of flash
sintering of strontium titanate were analyzed with different
acceptor dopant concentrations. The onset of flash sintering
was found to be dependent on the acceptor dopant
concentration, as expected by the increasing conductivity. A
gradient in the microstructure was found after flash
sintering with larger grain sizes at the negative electrode.
TEM-EDS measurements indicated Ti enrichment at the positive
electrode for undoped strontium titanate and strong acceptor
segregation for doped strontium titanate. In contrast, grain
boundaries at the negative electrode were found to be
stoichiometric for the undoped case and the acceptor
segregation was less obvious for the doped case.},
cin = {IEK-1},
ddc = {670},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {899 - ohne Topic (POF3-899)},
pid = {G:(DE-HGF)POF3-899},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000457665100036},
doi = {10.1016/j.actamat.2018.12.007},
url = {https://juser.fz-juelich.de/record/887826},
}