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@ARTICLE{Weidener:888282,
author = {Weidener, Dennis and Leitner, Walter and Domínguez de
María, Pablo and Klose, Holger and Grande, Philipp},
title = {{L}ignocellulose fractionation using recyclable phosphoric
acid: {L}ignin, cellulose and furfural production.},
journal = {ChemSusChem},
volume = {14},
number = {3},
issn = {1864-564X},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2020-04808},
pages = {909-916},
year = {2021},
abstract = {The conversion of lignocellulose into its building blocks
and their further transformation into valuable platform
chemicals (e.g. furfural) are key technologies to move
towards the use of renewable resources. This paper explores
the disentanglement of lignocellulose into
hemicellulose‐derived sugars, cellulose and lignin in a
biphasic solvent system (water/2‑methyltetrahydrofuran)
using phosphoric acid as recyclable catalyst. Integrated
with the biomass fractionation, in a second step
hemicellulose‐derived sugars – mainly xylose – are
converted to furfural, which is in situ extracted into
2‑methyltetrahydrofuran with high selectivity (70 $\%)$
and yield (56 $wt\%).$ To further increase the economic
feasibility of the process, a downstream and recycling
strategy enables recovery of phosphoric acid without loss of
process efficiency over four consecutive cycles. This
outlines a more efficient and sustainable use of phosphoric
acid as catalyst, as its inherent costs can be significantly
lowered.},
cin = {IBG-2},
ddc = {540},
cid = {I:(DE-Juel1)IBG-2-20101118},
pnm = {2172 - Utilization of renewable carbon and energy sources
and engineering of ecosystem functions (POF4-217)},
pid = {G:(DE-HGF)POF4-2172},
typ = {PUB:(DE-HGF)16},
pubmed = {33244874},
UT = {WOS:000596881900001},
doi = {10.1002/cssc.202002383},
url = {https://juser.fz-juelich.de/record/888282},
}