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@ARTICLE{Zheng:888819,
author = {Zheng, Fengshan and Kovács, András and Denneulin, Thibaud
and Caron, Jan and Weßels, Teresa and Dunin-Borkowski,
Rafal E.},
title = {{M}agnetic {F}ield {M}apping using {O}ff-{A}xis {E}lectron
{H}olography in the {T}ransmission {E}lectron {M}icroscope},
journal = {JoVE journal},
volume = {166},
issn = {1940-087X},
address = {Cambridge, MA},
publisher = {JoVE887169},
reportid = {FZJ-2020-05233},
pages = {e61907},
year = {2020},
abstract = {Off-axis electron holography is a powerful technique that
involves the formation of an interference pattern in a
transmission electron microscope (TEM) by overlapping two
parts of an electron wave, one of which has passed through a
region of interest on a specimen and the other is a
reference wave. The resulting off-axis electron hologram can
be analyzed digitally to recover the phase difference
between the two parts of the electron wave, which can then
be interpreted to provide quantitative information about
local variations in electrostatic potential and magnetic
induction within and around the specimen. Off-axis electron
holograms can be recorded while a specimen is subjected to
external stimuli such as elevated or reduced temperature,
voltage, or light. The protocol that is presented here
describes the practical steps that are required to record,
analyze, and interpret off-axis electron holograms, with a
primary focus on the measurement of magnetic fields within
and around nanoscale materials and devices. Presented here
are the steps involved in the recording, analysis, and
processing of off-axis electron holograms, as well as the
reconstruction and interpretation of phase images and
visualization of the results. Also discussed are the need
for optimization of the specimen geometry, the electron
optical configuration of the microscope, and the electron
hologram acquisition parameters, as well as the need for the
use of information from multiple holograms to extract the
desired magnetic contributions from the recorded signal. The
steps are illustrated through a study of specimens of
B20-type FeGe, which contain magnetic skyrmions and were
prepared with focused ion beams (FIBs). Prospects for the
future development of the technique are discussed.},
cin = {ER-C-1},
ddc = {610},
cid = {I:(DE-Juel1)ER-C-1-20170209},
pnm = {143 - Controlling Configuration-Based Phenomena (POF3-143)
/ 144 - Controlling Collective States (POF3-144) / 3D MAGiC
- Three-dimensional magnetization textures: Discovery and
control on the nanoscale (856538) / Q-SORT - QUANTUM SORTER
(766970) / ESTEEM3 - Enabling Science and Technology through
European Electron Microscopy (823717) / DARPA, Phase 2 -
Defense Advanced Research Projects Agency Manipulation of
magnetic skyrmions for logicin- memory applications
(Z1422.01.18) / DFG project 405553726 - TRR 270:
Hysterese-Design magnetischer Materialien für effiziente
Energieumwandlung (405553726)},
pid = {G:(DE-HGF)POF3-143 / G:(DE-HGF)POF3-144 /
G:(EU-Grant)856538 / G:(EU-Grant)766970 / G:(EU-Grant)823717
/ G:(DE-Juel-1)Z1422.01.18 / G:(GEPRIS)405553726},
typ = {PUB:(DE-HGF)16},
pubmed = {33346200},
UT = {WOS:000646166900037},
doi = {10.3791/61907},
url = {https://juser.fz-juelich.de/record/888819},
}