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@ARTICLE{RaviShankar:889850,
author = {Ravi Shankar, Sandheep and Garcia-Batlle, Marisé and
Bisquert, Juan and Garcia-Belmonte, Germà and Odrobina,
Jann and Schiller, Carl-Albrecht},
title = {{R}emoving {I}nstability-{C}aused {L}ow-{F}requency
{F}eatures in {S}mall {P}erturbation {S}pectra of
{P}erovskite {S}olar {C}ells},
journal = {The journal of physical chemistry / C},
volume = {124},
number = {29},
issn = {1932-7447},
address = {Washington, DC},
publisher = {Soc.},
reportid = {FZJ-2021-00458},
pages = {15793 - 15799},
year = {2020},
abstract = {Small-perturbation frequency-domain techniques such as
impedance spectroscopy and intensity-modulated photocurrent
spectroscopy (IMPS) have become important methods for the
investigation of the physical working mechanisms of the
perovskite solar cell (PSC). The validity of these methods
relies on assuming sample stability at the given steady
state. Through a series of IMPS measurements, we identify
that this assumption is invalid in certain cases for both
iodide and bromide-based PSCs that show strong time drift in
their IMPS response, noticeable in particular at low
frequencies, which are usually connected with the kinetics
of ionic motion and interaction with outer electrodes. Using
time course interpolation and a corrective Z-HIT algorithm
that connects the modulus of the IMPS transfer function and
its phase, we identify that the low-frequency arc/tail is in
certain cases an artifact generated by time drift of the
sample. Since the low-frequency data in an IMPS measurement
of the PSC provide important information regarding its
differential external quantum efficiency, care must be taken
to ascertain the origin and validity of the low-frequency
phenomena. Validity test is performed by using a combination
of corrective algorithms mentioned above and several
measurements over time to obtain stabilized spectra
virtually free of time drift.},
cin = {IEK-5},
ddc = {530},
cid = {I:(DE-Juel1)IEK-5-20101013},
pnm = {121 - Solar cells of the next generation (POF3-121)},
pid = {G:(DE-HGF)POF3-121},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000555507000013},
doi = {10.1021/acs.jpcc.0c04050},
url = {https://juser.fz-juelich.de/record/889850},
}