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@ARTICLE{Bernhard:890425,
author = {Bernhard, David and Kadyk, Thomas and Krewer, Ulrike and
Kirsch, Sebastian},
title = {{H}ow {P}latinum {O}xide {A}ffects the {D}egradation
{A}nalysis of {PEM} {F}uel{C}ell {C}athodes},
journal = {International journal of hydrogen energy},
volume = {46},
number = {26},
issn = {0360-3199},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2021-00945},
pages = {13791-13805},
year = {2021},
abstract = {In this work, proton exchange membrane fuel cell cathodes
are degraded with accelerated-stress-tests.These PtCo
containing cathodes are analyzed at begin-of-life and
end-of-test with a dedicated diagnostic procedure. For every
individual load point, the oxygen transport resistance and
voltage losses due to the formation of platinum oxides were
obtained in addition to commonly measured electrochemical
surface area, high frequency resistance, as well as cathode
ionomer resistance. These data were used to break down the
voltage losses into six different contributors. With this
break down, performance gains and performance losses were
determined at end-of-test. At low current densities, it was
found that voltage losses due to degradation are dominated
by the loss of specific activity and catalyst surface area -
in line with the state-of-the-art knowledge. But by
quantifying the losses from platinum oxide formation
explicitly, we show that end-of-test an unassigned voltage
loss is not only present at highest current densities, but
already at low current density. More precisely, the
unassigned voltage loss shows a linear increase with
decreasing half cell voltage and is independent from the
chosen accelerated stress test. As this unassigned loss
depends on half cell voltage, it might arise from ionomer
adsorption.},
cin = {IEK-13 / JARA-ENERGY},
ddc = {620},
cid = {I:(DE-Juel1)IEK-13-20190226 / $I:(DE-82)080011_20140620$},
pnm = {122 - Elektrochemische Energiespeicherung (POF4-122)},
pid = {G:(DE-HGF)POF4-122},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000636315800012},
doi = {10.1016/j.ijhydene.2021.01.058},
url = {https://juser.fz-juelich.de/record/890425},
}