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000891152 037__ $$aFZJ-2021-01400
000891152 1001_ $$0P:(DE-Juel1)173865$$aZeng, Fanlin$$b0$$eCorresponding author$$ufzj
000891152 245__ $$aMechanical reliability and oxygen permeationof Ce0.8Gd0.2O2-δ-FeCo2O4 dual phase membranes$$f - 2021-05-31
000891152 260__ $$aJülich$$bForschungszentrum Jülich GmbH Zentralbibliothek$$c2021
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000891152 4900_ $$aSchriften des Forschungszentrums Jülich Reihe Energie & Umwelt / Energy & Environment$$v529
000891152 502__ $$aDissertation, Univ. Twente, 2021$$bDissertation$$cUniv. Twente$$d2021
000891152 520__ $$aDual phase oxygen transport membranes, consisting of ionic and electronicconducting phases, exhibit great potential in high-purity oxygen generation due totheir high stability under harsh application atmospheres. Oxygen-ion conductivefluorite oxides (e.g. Ce0.8Gd0.2O2-δ) and electron conductive spinel phases (e.g.FeCo2O4) are promising material candidates for such a dual phase oxygen transportmembrane. Mechanical properties (e.g. elastic modulus, hardness, strength andsubcritical crack growth behaviour) and oxygen permeation of the membrane areimportant parameters regarding reliability for future applications. These parametershave close relationships with composition and microstructural characteristics, likegrain size, phase distribution and defects (e.g. microcracks). However, theserelationships are currently not fully understood. Therefore, in this thesis, theinfluence of composition, grain size and microstructural defects on mechanicalproperties are investigated for Ce0.8Gd0.2O2-δ-FeCo2O4 membranes. Millingprocedures during powder fabrication and ceramic sintering profiles are optimizedto overcome the formation of unfavorable microstructural defects ...
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