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@ARTICLE{Ruks:891697,
author = {Ruks, Tatjana and Loza, Kateryna and Heggen, Marc and
Prymak, Oleg and Sehnem, Andre Luiz and Oliveira, Cristiano
L. P. and Bayer, Peter and Beuck, Christine and Epple,
Matthias},
title = {{P}eptide-{C}onjugated {U}ltrasmall {G}old {N}anoparticles
(2 nm) for {S}elective {P}rotein {T}argeting},
journal = {ACS applied bio materials},
volume = {4},
number = {1},
issn = {2576-6422},
address = {Washington, DC},
publisher = {ACS Publications},
reportid = {FZJ-2021-01676},
pages = {945 - 965},
year = {2021},
abstract = {Ultrasmall gold nanoparticles with a metallic core diameter
of 2 nm were surface-conjugated with peptides that
selectively target epitopes on the surface of the WW domain
of the model protein hPin1 (hPin1-WW). The binding to the
gold surface was accomplished via the thiol group of a
terminal cysteine. The particles were analyzed by NMR
spectroscopy, high-resolution transmission electron
microscopy, and differential centrifugal sedimentation. The
surface loading was determined by conjugating a FAM-labeled
peptide, followed by UV–vis spectroscopy, and by
quantitative 1H NMR spectroscopy, showing about 150 peptide
molecules conjugated to each nanoparticle. The interaction
between the peptide-decorated nanoparticles with hPin1-WW
was probed by 1H–15N-HSQC NMR titration, fluorescence
polarization spectroscopy (FP), and isothermal titration
calorimetry (ITC). The particles showed a similar binding
(KD = 10–20 μM) compared to the dissolved peptides (KD =
10–30 μM). Small-angle X-ray scattering (SAXS) showed
that the particles were well dispersed and did not
agglomerate after the addition of hPin1-WW (no cross-linking
by the protein). Each nanoparticle was able to bind about 20
hPin1-WW protein molecules. An unspecific interaction with
hPin1 was excluded by the attachment of a nonbinding peptide
to the nanoparticle surface. The uptake by cells was studied
by confocal laser scanning microscopy. The
peptide-functionalized nanoparticles penetrated the cell
membrane and were located in the cytosol. In contrast, the
dissolved peptide did not cross the cell membrane.
Peptide-functionalized nanoparticles are promising agents to
target proteins inside cells.},
cin = {ER-C-1},
ddc = {570},
cid = {I:(DE-Juel1)ER-C-1-20170209},
pnm = {535 - Materials Information Discovery (POF4-535)},
pid = {G:(DE-HGF)POF4-535},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000643599900072},
doi = {10.1021/acsabm.0c01424},
url = {https://juser.fz-juelich.de/record/891697},
}