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001     891760
005     20240708133248.0
024 7 _ |a 10.1063/5.0012028
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100 1 _ |a Stadlmayr, Reinhard
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245 _ _ |a A high temperature dual-mode quartz crystal microbalance technique for erosion and thermal desorption spectroscopy measurements
260 _ _ |a [S.l.]
|c 2020
|b American Institute of Physics
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520 _ _ |a An improved quartz crystal microbalance measurement method is described, which allows us to determine erosion, implantation, and release rates of thin films, during changing temperatures and up to 700 K. A quasi-simultaneous excitation of two eigenmodes of the quartz resonator is able to compensate for frequency drifts due to temperature changes. The necessary electronics, the controlling behavior, and the dual-mode temperature compensation are described. With this improved technique, quantitative in situ temperature-programmed desorption measurements are possible and the quartz crystal microbalance can be used for quantification of thermal desorption spectroscopy measurements with a quadrupole mass spectrometer. This is demonstrated by a study of the retention and release behavior of hydrogen isotopes in fusion-relevant materials. We find that more than 90% of the deuterium implanted into a thin film of beryllium is released during a subsequent temperature ramp up to 500 K
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700 1 _ |a Szabo, Paul Stefan
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700 1 _ |a Biber, Herbert
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700 1 _ |a Koslowski, Hans Rudolf
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700 1 _ |a Kadletz, Elisabeth
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700 1 _ |a Cupak, Christian
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700 1 _ |a Wilhelm, Richard Arthur
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700 1 _ |a Schmid, Michael
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700 1 _ |a Linsmeier, Christian
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700 1 _ |a Aumayr, Friedrich
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773 _ _ |a 10.1063/5.0012028
|g Vol. 91, no. 12, p. 125104 -
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|t Review of scientific instruments
|v 91
|y 2020
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856 4 _ |y Published on 2020-12-03. Available in OpenAccess from 2021-12-03.
|u https://juser.fz-juelich.de/record/891760/files/5.0012028.pdf
856 4 _ |y Published on 2020-12-03. Available in OpenAccess from 2021-12-03.
|u https://juser.fz-juelich.de/record/891760/files/Postprint_Koslowski_A%20high%20temperature.pdf
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