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@ARTICLE{Svetlova:893127,
      author       = {Svetlova, Anastasia and Beltramo, Guillermo and Kireev,
                      Dmitry and Offenhäusser, Andreas},
      title        = {{Q}uartz crystal microbalance monitoring of large-area
                      graphene anodization reveals layer fracturing},
      journal      = {MRS advances},
      volume       = {6},
      number       = {10},
      issn         = {2059-8521},
      address      = {Cambridge},
      publisher    = {Cambridge University Press},
      reportid     = {FZJ-2021-02584},
      pages        = {270 - 275},
      year         = {2021},
      abstract     = {Graphene has numerous potential applications in ultrathin
                      electronics. There an electrode should function in contact
                      with fluids and under mechanical stress; therefore, its
                      stability is specifically of concern. Here, we explored a
                      custom-made quartz crystal microbalance (QCM) sensor covered
                      with wet-transferred large-scale monolayer graphene for
                      investigation of an electrode behavior. Monolayer graphene
                      was found to be stable on an oscillating substrate in
                      contact with air and liquid. Under the liquid flow and
                      simultaneously applied electrochemical potential, we managed
                      to induce graphene oxidation, impact of which was observed
                      on a quartz crystal microbalance monitoring and Raman
                      spectra. Applied potentials of 1 V and higher (vs. Ag/AgCl
                      reference electrode) caused graphene oxidation which led to
                      loss of the layer integrity and erosion of the material.},
      cin          = {IBI-2},
      ddc          = {670},
      cid          = {I:(DE-Juel1)IBI-2-20200312},
      pnm          = {524 - Molecular and Cellular Information Processing
                      (POF4-524)},
      pid          = {G:(DE-HGF)POF4-524},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000639706500001},
      doi          = {10.1557/s43580-021-00053-w},
      url          = {https://juser.fz-juelich.de/record/893127},
}