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@ARTICLE{Korte:893386,
author = {Korte, Carsten and Franz, Bernhard},
title = {{R}eaction kinetics in the system {Y}2{O}3/{A}l2{O}3 –
{A} solid state reaction forming multiple product phases
investigated by using thin film techniques},
journal = {Solid state ionics},
volume = {368},
issn = {0167-2738},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2021-02727},
pages = {115699 -},
year = {2021},
abstract = {The kinetics of the heterogeneous solid state reaction
between Al2O3 and Y2O3 is investigated by using thin film
techniques. Y2O3 films are grown by means of pulsed laser
deposition (PLD) on single crystalline alumina substrates
with a (0001) orientation. The solid state reactions are
performed at a temperature of 1400 °C (1673 K). The cross
sections of the reacted samples were investigated by means
of SEM and XRD and exhibit a sequence of three product
layers, Y3Al5O12 (YAG), YAlO3 (YAP) and Y4Al2O9 (YAM). The
simultaneous growth of the product layers is controlled by a
diffusional kinetics and the thickness increases are coupled
to each other. According to Wagner and Schmalzried, one has
to distinguish between rate constants of the first kind
(“practical” Tammann constant), in the case of
simultanous and coupled growth of multiple product phases,
and rate constants of the second kind (“true” Tammann
constant), in the case of the uncoupled and only growth of
one product phase in equilibrium with the adjacent phases.
The growth kinetics for a solid reaction forming three
product phases (layer) is analysed in detail using linear
transport theory. For the formation of YAG, YAP and YAM the
rate constants of the second kind are determined from the
experimental data and those of the first kind are calculated
and compared to the available literature data. Based on
these considerations, a detailed overview about the phase
formation kinetics in the temperature range of 1200–1400
°C can be given for the first time. The (Nernst-Planck
coupled) cation conductivities are calculated.},
cin = {IEK-14},
ddc = {530},
cid = {I:(DE-Juel1)IEK-14-20191129},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123)},
pid = {G:(DE-HGF)POF4-1231},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000681039300012},
doi = {10.1016/j.ssi.2021.115699},
url = {https://juser.fz-juelich.de/record/893386},
}