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@ARTICLE{Koch:893894,
author = {Koch, Julian and Müller-Caspary, Knut and Pfnür, Herbert},
title = {{M}atching different symmetries with an atomically sharp
interface: {E}pitaxial {B}a 2 {S}i{O} 4 on {S}i(001)},
journal = {Physical review materials},
volume = {4},
number = {1},
issn = {2475-9953},
address = {College Park, MD},
publisher = {APS},
reportid = {FZJ-2021-02906},
pages = {013401},
year = {2020},
abstract = {In this paper, we present a comprehensive investigation of
the epitaxial growth of Ba2SiO4 on Si(001), a system in
which neither crystal symmetry nor lattice constants match
in a simple manner. In addition, it has the potential to
become the first crystalline high-k gate dielectric. We
combined x-ray photoelectron spectroscopy, low-energy
electron diffraction, and aberration-corrected scanning
transmission electron microscopy (STEM) in order to optimize
the epitaxial growth by molecular beam epitaxy. Our focus
was on the formation of a high quality crystalline
interface. The films were grown by a co-deposition method
that requires no diffusion of Si from the substrate. An
annealing temperature of 400∘C turned out to be sufficient
to form chemically homogeneous films. However, crystalline
films require an annealing step to 670–690∘C for the
formation of the epitaxial interface necessary for breaking
Si-O bonds. STEM confirms that the interface is atomically
sharp and that a single layer of the silicate is changed to
a (2×3) structure at the interface from the (2×1.5) bulk
structure. Based on our experimental results, we propose a
geometrical model for the epitaxial interface. The growth of
films with an understoichiometric Si flux leads to the
formation of a near-surface Ba silicide that does not
restrict the epitaxial silicate growth.},
cin = {ER-C-1},
ddc = {530},
cid = {I:(DE-Juel1)ER-C-1-20170209},
pnm = {5351 - Platform for Correlative, In Situ and Operando
Characterization (POF4-535) / moreSTEM - Momentum-resolved
Scanning Transmission Electron Microscopy (VH-NG-1317)},
pid = {G:(DE-HGF)POF4-5351 / G:(DE-HGF)VH-NG-1317},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000506605500001},
doi = {10.1103/PhysRevMaterials.4.013401},
url = {https://juser.fz-juelich.de/record/893894},
}