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@ARTICLE{Meierhofer:893896,
author = {Meierhofer, Florian and Weigert, Florian and Dissinger,
Frank and Jungclaus, Jörgen and Müller-Caspary, Knut and
Waldvogel, Siegfried R. and Resch-Genger, Ute and Voss,
Tobias},
title = {{C}itric {A}cid {B}ased {C}arbon {D}ots with {A}mine {T}ype
{S}tabilizers: p{H}-{S}pecific {L}uminescence and {Q}uantum
{Y}ield {C}haracteristics},
journal = {The journal of physical chemistry / C},
volume = {124},
number = {16},
issn = {1932-7455},
address = {Washington, DC},
publisher = {Soc.},
reportid = {FZJ-2021-02908},
pages = {8894 - 8904},
year = {2020},
abstract = {We report the synthesis and spectroscopic characteristics
of two different sets of carbon dots (CDs) formed by
hydrothermal reaction between citric acid and
polyethylenimine (PEI) or 2,3-diaminopyridine (DAP).
Although the formation of amide-based species and the
presence of citrazinic acid type derivates assumed to be
responsible for a blue emission is confirmed for both CDs by
elemental analysis, infrared spectroscopy, and mass
spectrometry, a higher abundance of sp2-hybridized nitrogen
is observed for DAP-based CDs, which causes a red-shift of
the n-π* absorption band relative to the one of PEI-based
CDs. These CD systems possess high photoluminescence quantum
yields (QY) of $∼40\%$ and $∼48\%$ at neutral pH,
demonstrating a possible tuning of the optical properties by
the amine precursor. pH-Dependent spectroscopic studies
revealed a drop in QY to < $9\%$ (pH ∼ 1) and < $21\%$ (pH
∼ 12) for both types of CDs under acidic and basic
conditions. In contrast, significant differences in the
pH-dependency of the n-π* transitions are found for both CD
types which are ascribed to different (de)protonation
sequences of the CD-specific fluorophores and functional
groups using zeta potential analysis.},
cin = {ER-C-1},
ddc = {530},
cid = {I:(DE-Juel1)ER-C-1-20170209},
pnm = {5351 - Platform for Correlative, In Situ and Operando
Characterization (POF4-535) / moreSTEM - Momentum-resolved
Scanning Transmission Electron Microscopy (VH-NG-1317)},
pid = {G:(DE-HGF)POF4-5351 / G:(DE-HGF)VH-NG-1317},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000529225800047},
doi = {10.1021/acs.jpcc.9b11732},
url = {https://juser.fz-juelich.de/record/893896},
}